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Heating type electro-chemical trace amount detection pool integrated on conductive glass

A conductive glass and detection cell technology, applied in the direction of material electrochemical variables, etc., can solve the problems of aggravating waste liquid pollution, refractory solution, environment, etc., to achieve elimination of adsorption phenomenon, sensitive electrolytic current, and good detection reproducibility Effect

Inactive Publication Date: 2009-07-15
FUZHOU UNIV
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The three-electrode system of the traditional electrochemiluminescence detection cell has a large size and poor integration, and the volume of the required electrolyte solution is large, which not only wastes analytical reagents, increases the cost of the experiment, but also increases the environmental pollution of the waste liquid after the experiment.
At present, electrochemical researchers at home and abroad have made various attempts to integrate the three-electrode system, mainly to develop printed electrodes based on carbon and gold materials, and to a certain extent have realized the integration of the three-electrode system, but so far the printed electrode The production process is relatively complicated and the reproducibility is poor. The production process uses precious metals such as silver and gold, and the cost is relatively high, which limits the promotion of printed electrodes.
In addition, printed electrodes are basically made of disposable type, that is, they are discarded after the experiment is completed. However, since the matrix materials of printed electrodes are mostly plastics that are difficult to decompose, a large amount of discarding will inevitably cause severe environmental problems.

Method used

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  • Heating type electro-chemical trace amount detection pool integrated on conductive glass
  • Heating type electro-chemical trace amount detection pool integrated on conductive glass
  • Heating type electro-chemical trace amount detection pool integrated on conductive glass

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Embodiment Construction

[0010] Embodiments of the present invention will be further described below in conjunction with the accompanying drawings.

[0011] As shown in the figure, the heating type electrochemical micro detection cell integrated on the conductive glass of the present invention includes a conductive glass with a conductive layer on the surface, the conductive glass includes a glass matrix 2 and a conductive layer 1, and is characterized in that: the conductive glass The conductive layer is etched with acid to form three parts insulated from each other, which are respectively used as the working electrode 6, the auxiliary electrode 4 and the reference electrode 3 to form a full ITO three-electrode system; wherein the ITO working electrode is connected to the heating circuit 8 to realize the working electrode. Heating; the top of the ITO three-electrode system is covered with an insulating thin layer 7, and the insulating thin layer is provided with a three-electrode connection port 9 and...

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Abstract

The present invention relates to a heating type electrochemical trace detection pool integrated on a conductive glass, comprising a conductive glass with a conductive layer on the surface, characterized in that: the conductive layer of the conductive glass is subjected to acid etching into three parts which are isolated from each other, respectively as a working electrode, an auxiliary electrode and a reference electrode to form a full ITO three-electrode system; wherein the ITO working electrode is connected with a heating circuit to raising the temperature of the working electrode; an insulation thin layer is covered above the ITO three-electrode system and a tree-electrode connection port and a detection pool port are provided on the insulation thin layer and a sealing cam for blocking the edge of the detection pool is set between the lower side of the insulation thin layer and the edge of the detection pool. The detection pool has features of high integration degree, compactness, simple manufacture technique, low cost and repeated use.

Description

technical field [0001] The invention relates to a heating type electrochemical micro detection cell integrated on conductive glass. technical background [0002] The electrochemical detection cell is a device used to detect and study the electrochemical activity of substances. It is generally composed of a three-electrode system composed of a working electrode, an auxiliary electrode and a reference electrode, and an appropriate amount of electrolyte solution. The three-electrode system of the traditional electrochemiluminescence detection cell has a large size and poor integration, and the volume of the electrolyte solution required is large, which not only wastes analytical reagents, increases the cost of the experiment, but also increases the environmental pollution of the waste liquid after the experiment. At present, electrochemical researchers at home and abroad have made various attempts to integrate the three-electrode system, mainly to develop printed electrodes bas...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N27/28
Inventor 池毓务陈丽婵陈国南
Owner FUZHOU UNIV
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