Mn-Zn ferrite magnetic material with high magnetoconductivity and high impedance and method for making the same
A technology of magnetic material and high magnetic permeability, applied in the field of Mn-Zn ferrite magnetic material, Mn-Zn ferrite magnetic material and its preparation field, can solve the problem of poor resistance characteristic of Mn-Zn ferrite magnetic material and other problems, to achieve the effect of high permeability, stable process and low production cost
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Embodiment 1
[0023] 1. Ingredients: according to the weight percentage of the main formula and auxiliary formula in terms of oxides, the main formula is Fe 2 o 3 is 61wt%; ZnO is 28wt%; Mn 3 o 4 is 11wt%; the auxiliary formula is CaCO 3 : 50ppm, SiO 2 : 80ppm, Bi 2 o 3 : 100ppm, MoO 3 : 400ppm.
[0024] 2. Ball milling: dry strong mixing with a V-shaped mixer, and the mixing time is 0.7 hours;
[0025] 3. Vibration grinding: Vibration grinding machine is used for vibration grinding, and the vibration grinding time is 0.6 hours;
[0026] 4. Pre-burning: The powder is directly pre-fired in an air kiln at a temperature of 600°C for 10 hours.
[0027] 5. Sanding, spray granulation, forming: use a circulating sand mill for sanding, and the sanding time is 2 hours; wherein the material: ball: water = 1:1:0.6; the average particle size of the powder after sanding It is 1.0~1.2μm. After sanding, use a spray granulator to granulate, and then use a fully automatic dry press to shape.
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Embodiment 2
[0030] 1. Ingredients: according to the weight percentage of the main formula and auxiliary formula in terms of oxides, the main formula is Fe 2 o 3 69wt%; ZnO 15.5wt%; Mn 3 o 4 is 15.5wt%; the auxiliary formula is CaCO 3 : 100ppm, SiO 2 : 60ppm, Bi 2 o 3 : 250ppm, MoO 3 : 200ppm, Nb 2 o 5 100ppm, TiO 2 is 250ppm.
[0031] 2. Ball milling: dry strong mixing with a V-shaped mixer, and the mixing time is 0.7 hours;
[0032] 3. Vibration grinding: Vibration grinding machine is used for vibration grinding, and the vibration grinding time is 0.6 hours;
[0033] 4. Pre-burning: The powder is directly pre-fired in an air kiln at a temperature of 950°C for 3 hours.
[0034] 5. Sanding, spray granulation, forming: use a circulating sand mill for sanding, and the sanding time is 2 hours; wherein the material: ball: water = 1:1:0.6; the average particle size of the powder after sanding It is 1.0~1.2μm. After sanding, use a spray granulator to granulate, and then use a fully ...
Embodiment 3
[0037] 1. Ingredients: according to the weight percentage of the main formula and auxiliary formula in terms of oxides, the main formula is Fe 2 o 3 is 72wt%; ZnO is 12wt%; Mn 3 o 4 is 16wt%; the auxiliary formula is CaCO 3 : 300ppm, SiO 2 : 200ppm, Bi 2 o 3 : 400ppm, MoO 3 : 100ppm, Nb 2 o 5 150ppm, TiO 2 150ppm.
[0038] 2. Ball milling: dry strong mixing with a V-shaped mixer, and the mixing time is 0.7 hours;
[0039] 3. Vibration grinding: Vibration grinding machine is used for vibration grinding, and the vibration grinding time is 0.6 hours;
[0040] 4. Pre-burning: The powder is directly pre-fired in an air kiln at a temperature of 1200°C for 1 hour.
[0041] 5. Sanding, spray granulation, forming: use a circulating sand mill for sanding, and the sanding time is 2 hours; wherein the material: ball: water = 1:1:0.6; the average particle size of the powder after sanding It is 1.0~1.2μm. After sanding, use a spray granulator to granulate, and then use a fully ...
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