Bamboo pupa protein fiber long-short yarn and method for making same
A protein fiber, silkworm chrysalis protein technology, applied in the direction of cellulose/protein conjugated rayon, fiber processing, short fiber formation, etc., to achieve the effects of stable supply and spinning pressure, fast moisture release, and excellent heat exchange effect.
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Embodiment 1
[0031] Embodiment 1 Preparation of bamboo pupa protein fiber filament of the present invention
[0032] a, prepare silkworm chrysalis protein spinning solution, defoaming;
[0033] The preparation method of step a silkworm chrysalis protein spinning solution is as follows:
[0034] (1), get silkworm chrysalis protein 10kg and sodium hydroxide 0.6kg;
[0035] (2), dissolving silkworm chrysalis protein in the sodium hydroxide aqueous solution that temperature is 45 ℃, and concentration is 0.6%w / w, obtains silkworm chrysalis protein solution through filtration;
[0036] (3), get silkworm chrysalis protein solution (wherein containing silkworm chrysalis protein 1kg), 0.08kg of acrylamide by following solid weight, carry out carbamoyl ethylation reaction, filter, obtain silkworm chrysalis protein spinning solution.
[0037] b. Bamboo cellulose is extracted from bamboo;
[0038] It is prepared by chemical and physical methods to remove impurities in bamboo through multiple proces...
Embodiment 2
[0044] The preparation of embodiment 2 bamboo pupa protein fiber short filaments of the present invention
[0045] Steps a to d are the same as in Example 1, and step e is as follows: the fiber tow described in step d is drawn in a bundle, and then enters into plasticizing and stretching, and the cut length is 38-76 mm; It is evenly spread on the fourdrinier wire surface, and as the fourdrinier wire moves forward, hydroformylation, pickling, desulfurization, water washing, oiling and drying are respectively completed in each section to obtain the bamboo fibrin short filaments of the present invention.
Embodiment 3
[0046] The preparation of embodiment 3 bamboo pupa protein fiber filament of the present invention
[0047] a, prepare silkworm chrysalis protein spinning solution, defoaming;
[0048] The preparation method of step a silkworm chrysalis protein spinning solution is as follows:
[0049] (1), get silkworm chrysalis protein 10kg and sodium hydroxide 1.5kg;
[0050] (2), dissolving silkworm chrysalis protein in the sodium hydroxide aqueous solution that temperature is 70 ℃, and concentration is 2%w / w, obtains silkworm chrysalis protein solution through filtration;
[0051] (3), get silkworm chrysalis protein solution (wherein containing silkworm chrysalis protein 1kg), acrylamide 0.18kg by following solid weight, carry out carbamoyl ethylation reaction, filter, obtain silkworm chrysalis protein spinning solution.
[0052] b. Bamboo cellulose is extracted from bamboo;
[0053] It is prepared by chemical and physical methods to remove impurities in bamboo through multiple process...
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