Method for preparing carbon covered nickel nano grain enhanced silver based composite material
A nano-particle, carbon-coated nickel technology, applied in metal material coating process, gaseous chemical plating, coating and other directions, can solve problems such as uneven dispersion of reinforcement phase, achieve a simple and convenient preparation method, and is conducive to comprehensive performance , the effect of good electrical performance
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Embodiment 1
[0030] The first step, preparation of Ni+Ag catalyst precursor NiO+Ag by deposition-precipitation method 2 o
[0031] Add nickel nitrate hexahydrate and silver nitrate into deionized water at a mass ratio of 0.03:1 to prepare an aqueous solution with a molar concentration of nickel nitrate of 0.01mol / L and simultaneously contain nickel ions and silver ions, and add dropwise to the solution Molar concentration is 1.25mol / L sodium hydroxide solution to pH value is 10, and is precipitated, makes the Ni(OH) of mass ratio Ni:Ag=0.01:1 2 +Ag 2 O binary colloid, the Ni(OH) 2 +Ag 2 The O binary colloid was put into an electric constant temperature drying oven, dehydrated to complete dryness at 250 °C and nitrogen atmosphere, and then placed in a tube furnace for calcination at 300 °C for 3 hours to obtain the Ni+Ag catalyst precursor NiO+Ag 2 O powder;
[0032] The second step is to prepare carbon-coated nickel nanoparticles + silver in-situ composite powder by chemical vapor dep...
Embodiment 2
[0037] The first step, preparation of Ni+Ag catalyst precursor NiO+Ag by deposition-precipitation method 2 o
[0038] With embodiment 1;
[0039] The second step is to prepare carbon-coated nickel nanoparticles + silver in-situ composite powder by chemical vapor deposition
[0040] Except that the catalytic cracking reaction time is 2h, the carbon-coated nickel nanoparticles + silver in-situ composite powder with an average particle size of 28nm is obtained, and the yield of carbon-coated nickel nanoparticles is 0.31%, other processes, conditions and results Same as embodiment 1;
[0041] The third step is to prepare carbon-coated nickel nanoparticles reinforced silver-based composites
[0042] With embodiment 1.
[0043] The high-resolution scanning electron micrograph of the carbon-coated nickel nanoparticles + silver in-situ composite powder obtained in this example is shown in figure 1 , where the high-resolution transmission electron micrographs of carbon-coated nick...
Embodiment 3
[0046] The first step, preparation of Ni+Ag catalyst precursor NiO+Ag by deposition-precipitation method 2 o
[0047] Add nickel nitrate hexahydrate and silver nitrate into deionized water at a mass ratio of 0.17:1 to prepare an aqueous solution containing nickel ions and silver ions with a molar concentration of nickel nitrate of 0.04 mol / L, and add dropwise to the solution Molar concentration is 1.25mol / L sodium hydroxide solution to pH value is 10, and is precipitated, makes the Ni(OH) of mass ratio Ni:Ag=0.05:1 2 +Ag 2 O binary colloid, the Ni(OH) 2 +Ag 2 The O binary colloid was put into an electric constant temperature drying oven, dehydrated to complete dryness at 150 °C and nitrogen atmosphere, and then placed in a tube furnace for calcination at 400 °C for 2 hours to obtain the Ni+Ag catalyst precursor NiO+Ag 2 O powder;
[0048] The second step is to prepare carbon-coated nickel nanoparticles + silver in-situ composite powder by chemical vapor deposition
[004...
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