Catalytic distillation tower reaction segment structrue
A technology of catalytic distillation tower and reaction section, which is applied in the field of catalyst filling method in catalytic distillation tower, and can solve the problems of increased resistance of liquid phase materials flowing through the catalyst bed layer, affecting catalyst reaction efficiency, and large radial size, etc.
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[0041] Attached according to the invention figure 1 And attached figure 2 The structure scheme of the reaction section shown is used for the dehydration of methanol to dimethyl ether. The catalytic distillation tower is composed of a rectification section, a reaction section, and a stripping section. In the reaction section, a layer of separation trays is set between every two catalyst trays. Methanol The conversion rate reaches 97%, the selectivity of dimethyl ether reaches 99.99%, and the purity of the dimethyl ether product reaches 99.9%. The unreacted methanol and the water generated by the reaction are discharged from the tower kettle together, and then recycled and reacted.
[0042] Operating conditions:
[0043] The number of catalyst beds in the reaction section of the catalytic distillation tower, 15
[0044] Catalytic distillation tower top pressure, 2.0MPa
[0045] Methanol volumetric space velocity, 1.0h -1
[0046] Catalytic distillation column reflux ratio,...
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