Process for preparing organic phase-change material composite expanded perlite by emulsification method
A technology for the preparation of expanded perlite, which is applied in the field of building energy conservation, can solve the problems of affecting the mechanical properties of building materials, worrying about the practical prospect, and affecting the fire performance of products, so as to facilitate the promotion and application of industrialization, easy implementation and control, and high phase change The effect of energy storage heat capacity
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Embodiment 1
[0021] 20kg of paraffin, 100kg of water, and 10kg of paraffin emulsifier (produced by Haian Petrochemical Factory in Jiangsu Province). Preparation process: Heat the water to 80°C, add the measured paraffin emulsifier to the measured paraffin, mix and heat to melt, then add this mixture to the above hot water and stir evenly, keep it warm for 1 hour, and cool to form a paraffin emulsion. Then, the emulsified organic phase change material is completely adsorbed and infiltrated into the expanded perlite by using a decompression adsorption process, and the organic phase change material composite expanded perlite particles are obtained. The decompression adsorption process is as follows: put the above-mentioned paraffin emulsion and 100kg of expanded perlite particles with a diameter of 4mm into a vacuum stirring pot, and vacuumize while stirring, and the vacuum degree reaches 9.8×10 -2 Pa hold it for 3 minutes, then slowly release the pressure to normal pressure, repeat the above...
Embodiment 2
[0024] Fatty acid 50kg, sodium dodecyl sulfate 10kg, water 100kg. Preparation process: Heat water to 80°C, mix fatty acid and sodium dodecylsulfonate and heat to melt, then add this mixture into the above hot water and stir evenly, keep warm for 2 hours, and cool to form an emulsion. Then, the emulsified organic phase change material is completely adsorbed and infiltrated into the expanded perlite by using a decompression adsorption process, and the organic phase change material composite expanded perlite particles are obtained. The decompression adsorption process is as follows: put the above-mentioned emulsion and 100kg of expanded perlite particles with a diameter of 8mm into a vacuum stirring pot, and vacuumize while stirring, and the vacuum degree reaches 9.8×10 -2 Pa hold it for 3 minutes, then slowly release the pressure to normal pressure, repeat the above vacuuming and pressure relief process twice, and let the material dry naturally, that is, the organic phase change...
Embodiment 3
[0027] 100kg of n-dodecane, 80kg of monooleate, and 200kg of water. Preparation process: heat water to 80°C, mix n-dodecane and monooleate and heat to melt, then add this mixture into the above-mentioned hot water and stir evenly, keep it warm for 4 hours, and cool to form an emulsion. Then, the emulsified organic phase change material is completely adsorbed and infiltrated into the expanded perlite by using a decompression adsorption process, and the organic phase change material composite expanded perlite particles are obtained. The decompression adsorption process is as follows: put the above emulsion and 200kg of expanded perlite particles with a diameter of 6mm into a vacuum stirring pot, and vacuumize while stirring, and the vacuum degree reaches 9.8×10 -2 Pa hold it for 3 minutes, then slowly release the pressure to normal pressure, repeat the above vacuuming and pressure relief process twice, and let the material dry naturally, that is, the organic phase change materia...
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