Process for synthesizing sec-butyl urea
A technology for sec-butyl urea and sec-butyl amine, which is applied in the field of synthesizing sec-butyl urea by a CO2 catalytic method, can solve the problems of low market value and high cost of potassium sulfate, and achieve the effects of high market value, simple method and cost reduction.
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Embodiment 1
[0021] Dilute 8.2g of sec-butylamine with 45ml of water and put it in a four-necked flask, weigh 8.1g of potassium cyanate and dissolve it in 20ml of water, add it to the four-necked flask, stir and mix well. Infuse CO under normal pressure 2 gas, maintained at 30°C for 4 hours. Evaporate water and excess sec-butylamine, add 50ml of ethanol, filter while hot to obtain 4.5g of by-product potassium carbonate, evaporate and concentrate the filtrate to obtain 7.6g of product sec-butylurea, and the conversion rate per pass is 65.2%.
Embodiment 2
[0023] Dilute 7.3g of sec-butylamine with 20ml of water and put it in a four-necked flask, weigh 8.1g of potassium cyanate and dissolve it in 20ml of water, add it to the four-necked flask, stir and mix well. Infuse CO under normal pressure 2 gas, maintained at 55°C for 6 hours. Evaporate water and excess sec-butylamine, add 50ml of ethanol, filter while hot to obtain 3.8g of by-product potassium carbonate, and evaporate and concentrate the filtrate to obtain 6g of product sec-butylurea, with a single-pass conversion rate of 51.7%.
Embodiment 3
[0025] Dilute 8.2g of sec-butylamine with 30ml of water and put it in a four-necked flask, weigh 8.1g of potassium cyanate and dissolve it in 20ml of water, add it to the four-necked flask, stir and mix well. Inject CO at 10 atmospheres 2 gas, maintained at 60°C for 3 hours. The water and excess sec-butylamine were distilled off, 50 ml of methanol was added, and 5.6 g of by-product potassium carbonate was obtained by filtration while hot, and the filtrate was evaporated and concentrated to obtain 9.63 g of the product sec-butylurea, with a one-pass conversion rate of 83.0%.
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