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Spherical high pressure multiple phase reactor

A multi-phase reactor and reactor technology, which is applied to pressure vessels used in chemical processes and other directions, can solve the problems of harsh wall thickness and material selection requirements, infeasible mechanical and design processing, and low interphase mass transfer efficiency. Improve fluid short-circuit or uneven distribution, enhance contact and mixing, and prevent dead zones

Inactive Publication Date: 2005-03-02
TSINGHUA UNIV
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Problems solved by technology

At present, the more advanced reactors in these industrial processes generally adopt the gas-liquid-solid three-phase slurry operating system. The slurry bed reactor has the characteristics of excellent heat transfer performance, but the mass transfer efficiency between phases is relatively low, resulting in industrially designed reactions. The volume of the reactor is relatively large, and to achieve economically profitable large-scale design, the volume of the reactor will also be larger
The high-pressure operation of the system has very strict requirements on the wall thickness and material selection of the reactor, especially for large-scale high-pressure reactors such as cylindrical vessels with a diameter of about 10 meters.

Method used

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Embodiment Construction

[0013] The invention provides a spherical high-pressure multiphase reactor. This spherical high-pressure multiphase reactor is a kind of gas-liquid or gas-liquid solid-slurry state spherical reactor, and this reactor is formed by connecting pipe 12 in series by lower spherical container 3 and upper spherical container 6 or a plurality of spherical containers (as figure 1 As shown), the gas distributor 2 is fixed on the bottom of the lower spherical container 3, the internal partition baffle 13 of the spherical container is supported above the gas distributor 2 in the lower spherical container 3, and the multi-layer interlaced inner member 10 is fixed on the internal partition baffle of the spherical container In the plate 13, the internal member 11 with the central blunt body diversion function is directly fixed on the mouth connecting the upper spherical container 6 and the lower spherical container 3, the swirl plate 7 and the gas-liquid separator 8 are arranged at the outlet...

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Abstract

The spherical high-pressure multiple phase reactor is one chemical apparatus for gas-liquid or gas-liquid-solid slurry reaction. The reactor consists of two or more spherical reactors connected serially. It has gas distributor fixed in the bottom of the lower spherical container, separating baffles supported inside the spherical container, and laminated inner members fixed inside the separating baffles for realizing the homogeneous phase distribution of the gas phase in different spherical parts of different cross section areas to promote the homogeneous distribution and raised contact efficiency of different phases. The inner members have functions of guiding flow, re-distributing and inhibiting bubble growth. Compared with cylindrical reactor, the present invention has one half reduced wall thickness, easy construction and reduced investment, and is suitable for large high pressure reaction process.

Description

technical field [0001] The invention belongs to the scope of chemical equipment, in particular to a spherical high-pressure multiphase reactor. Background technique [0002] Chemical and petrochemical processes involve a large number of high-pressure multiphase reaction processes, such as petroleum hydrocracking, methanol synthesis, Fischer-Tropsch synthesis, dimethyl ether synthesis and other energy-related industrial processes. These processes are related to the national energy strategy. Feasibility depends on the scale of production. If it is necessary to build a single device with a production capacity of hundreds of thousands of tons of reactors, due to the requirements of high-pressure processes and industrial scale-up, the traditional cylindrical reactors face design difficulties. At present, the more advanced reactors in these industrial processes generally adopt the gas-liquid-solid three-phase slurry operating system. The slurry bed reactor has the characteristics...

Claims

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Application Information

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IPC IPC(8): B01J3/04
Inventor 程易王金福金涌杜闰萍
Owner TSINGHUA UNIV
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