Extracting and preparing process for Echinacea prupurea and its products
A technology of echinacea purpurea extract and extraction process, which is applied in medical preparations containing active ingredients, separation/purification of carboxylic acid esters, organic chemistry, etc., can solve the problems that the extraction process of echinacea purpurea extract has not been reported, and achieve low cost , production safety, high-purity effect
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Embodiment 1
[0018] Take 20 grams of Echinacea plant powder as raw material, place it in a round-bottomed flask, add 10 times (ie 200ml) 30% ethanol solution (add quantitative enzyme inhibitor), place on a water bath, reflux and extract at 55℃ After 2 hours, the filtrate and residue were collected after filtration. Then add 10 times the 30% ethanol solution to the residue, reflux and extract for 2 hours under the same conditions, then filter, and combine the two filtrates. Place the filtrate at 4°C for 24 hours, then filter to remove the precipitate, and then pass through a 0.45um microporous membrane to remove bacteria and macromolecular proteins. The filtrate from which the protein has been removed is placed on a rotary evaporator, concentrated by rotary evaporation at 50°C, and concentrated until thick and strong, and then evaporated to a paste in a water bath at 70°C. Finally, the concentrated extract is placed in a vacuum drying oven and dried under vacuum at 50-60°C. The brown solid extr...
Embodiment 2
[0020] Take 20 grams of Echinacea plant powder as raw material, place it in a round-bottomed flask, add 15 times (ie 300ml) 40% ethanol solution, place it on a water bath, reflux and extract at 70℃ for 4 hours, filter and collect the filtrate and Residue. Then add 15 times the 40% ethanol solution to the residue, reflux and extract for 4 hours under the same conditions, then filter, and combine the two filtrates. Place the filtrate at 4°C for 24 hours, then filter to remove the precipitate, and then pass through a 0.45um microporous membrane to remove bacteria and macromolecular proteins. The filtrate from which the protein has been removed is placed on a rotary evaporator, concentrated by rotary evaporation at 50°C, and concentrated until thick and strong, and then evaporated to a paste in a water bath at 70°C. Finally, the concentrated extract is placed in a vacuum drying oven and dried under vacuum at 50-60°C. The brown solid extract can be obtained. The extract is dissolved, a...
Embodiment 3
[0022] Take 20 grams of Echinacea plant powder as raw material, place it in a round bottom flask, add 15 times (ie 300ml) 80% ethanol solution, place it on a water bath, reflux for 2 hours at 55℃, collect the filtrate and Residue. Then add 15 times the 80% ethanol solution to the residue, reflux and extract for 2 hours under the same conditions, then filter, and combine the two filtrates. Place the filtrate at 4°C for 24h, then filter to remove the precipitate, and then pass through a 0.45um microporous membrane to remove bacteria and macromolecular proteins. The filtrate from which the protein has been removed is placed on a rotary evaporator, concentrated by rotary evaporation at 50°C, and concentrated until thick and strong, and then evaporated to a paste in a water bath at 70°C. Finally, the concentrated extract is placed in a vacuum drying oven and dried under vacuum at 50-60°C. The brown solid extract can be obtained. The extract is dissolved, and the analysis result of high...
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