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Graphene oxide waste conversion and recovery device and method thereof

A technology of a recovery device and a recovery method, applied in the field of graphene oxide waste conversion and recovery devices, can solve the problems of large cleaning water consumption, high slurry viscosity, difficult solid content, etc., and achieves improved processing efficiency, simple operation method, and accelerated reduction. effect of reaction

Pending Publication Date: 2022-05-24
SUZHOU SIDIKE NEW MATERIALS SCI & TECH
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Problems solved by technology

Due to the problems of unstable properties, difficult determination of solid content, high viscosity of slurry, poor consistency and high water consumption for cleaning of graphene oxide waste, the cost of graphene oxide waste treatment is relatively high and the treatment has certain pollution.
At present, the general treatment methods of graphene oxide waste include: flocculant flocculation treatment and reducing agent reduction treatment. The above methods have problems such as high cost, unfriendly to the environment, secondary pollution, difficult recycling and complicated post-treatment.

Method used

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  • Graphene oxide waste conversion and recovery device and method thereof

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Embodiment 1

[0071] The present embodiment provides a graphene oxide waste conversion and recovery method. Use the graphene oxide waste conversion and recovery method of the above-mentioned graphene oxide waste conversion and recovery device 10, comprising the steps:

[0072]Step 1: Add graphene oxide slurry to the cathode reaction chamber 210 , and add water to the anode reaction chamber 110 . The height of adding water into the anode reaction chamber 110 does not exceed 2 / 3 of the height of the inner wall of the anode reaction chamber 110 . When the graphene oxide slurry is solid, the graphene oxide waste is soaked for 3-12 hours before being added to the cathode reaction chamber 210 .

[0073] Step 2: Control the second electrode 220 to rotate at a speed of 50 rpm.

[0074] Step 3: Connect the first electrode 120 to the positive pole of the power supply, connect the second electrode 220 to the cathode of the power supply, and use a direct current with a voltage of 0.5-3V to carry out ...

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Abstract

The invention discloses a graphene oxide waste conversion and recovery device and a method thereof. The graphene oxide waste conversion and recovery device comprises an anode reaction assembly and a cathode reaction assembly, the anode reaction assembly comprises an anode reaction chamber and a first electrode, the first electrode is installed in the anode reaction chamber and used for being connected with a power source anode, and the cathode reaction assembly comprises a cathode reaction chamber and a second electrode. The second electrode is installed in the cathode reaction chamber and used for being connected with a power source cathode. According to the graphene oxide waste conversion and recovery device, graphene waste recovery is achieved through an electrochemical method, on one hand, dispersed high-viscosity graphene oxide is efficiently converted and recovered into self-agglomerated and easily-separated graphene; on the other hand, any other chemical medicine is not needed, harmful substances to the environment are not generated, green and pollution-free effects are achieved, and the problems of high cost, environmental unfriendliness, secondary pollution, difficulty in recovery, complicated post-treatment and the like of a chemical treatment method in the traditional technology are solved.

Description

technical field [0001] The invention relates to the field of graphene waste treatment, in particular to a graphene oxide waste conversion and recovery device and a method thereof. Background technique [0002] With the increasing application of graphene oxide, a large amount of graphene oxide waste (including sewage) will inevitably be generated during the large-scale production of graphene oxide. Due to the unstable properties of graphene oxide waste, difficult determination of solid content, high slurry viscosity, poor consistency, and large cleaning water consumption, the cost of graphene oxide waste treatment is relatively high and the treatment has certain pollution. At present, the general treatment methods of graphene oxide waste include: flocculant flocculation treatment and reducing agent reduction treatment. The above methods have problems such as high cost, unfriendly to the environment, secondary pollution, difficult recovery and complex post-processing. SUMMAR...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C25B1/135C25B1/50C01B32/184
CPCC25B1/135C25B1/50C01B32/184Y02E60/50
Inventor 金闯胡浩周亮
Owner SUZHOU SIDIKE NEW MATERIALS SCI & TECH
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