A kind of preparation method of cinnamon extract and its cinnamon extract and application
A cinnamon extract and cinnamon technology, which is applied in the preparation of cinnamon extract, cinnamon extract and its application in lowering blood sugar, can solve the problems of cinnamon extract being volatile at high temperature and low extraction rate, achieve safety and side effects, and improve extraction rate, wide-ranging effects
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Embodiment 1
[0036] Select 1 kg of high-quality cinnamon medicinal material and pulverize it with a pulverizer. Take 50 g of cinnamon powder, put it in a clean beaker, and soak it in 400 mL of ethanol and water composite solvent (75% ethanol volume fraction) for 30 min. After soaking, adjust the pH of the solution to 5 with hydrochloric acid, put it into an ultrasonic instrument for ultrasonic extraction, 45 ° C, 500 W, ultrasonic extraction for 30 min, filter under reduced pressure to separate the extract and cinnamon solid, and put the cinnamon solid in the original beaker again According to the solid-liquid ratio of 1:8g / mL, add ethanol-water composite solvent (ethanol volume fraction 75%), adjust the pH of the solution to 3 with hydrochloric acid, put it into an ultrasonic instrument for extraction, 45 ° C, 500 W, ultrasonic extraction After 30 min of extraction, filter under reduced pressure to separate the extract from the cinnamon solid, collect the extract, and discard the cinnamon...
Embodiment 2
[0038] Select 1 kg of high-quality cinnamon medicinal material and pulverize it with a pulverizer. Take 50 g of cinnamon powder, put it in a clean beaker, and soak it in 500 mL of ethanol and water composite solvent (55% ethanol volume fraction) for 30 min. After soaking, adjust the pH of the solution to 6 with hydrochloric acid, put it into an ultrasonic instrument for ultrasonic extraction, 55 ° C, 400 W, ultrasonic extraction for 30 min, filter under reduced pressure to separate the extract and cinnamon solid, and put the cinnamon solid in the original beaker again According to the solid-liquid ratio of 1:10g / mL, add ethanol-water composite solvent (55% ethanol volume fraction), adjust the pH of the solution to 4 with hydrochloric acid, put it into an ultrasonic instrument for extraction, 55 ° C, 400 W, ultrasonic extraction After 30 min of extraction, filter under reduced pressure to separate the extract from the cinnamon solid, collect the extract, and discard the cinnamo...
Embodiment 3
[0040]Select 1 kg of high-quality cinnamon medicinal material and pulverize it with a pulverizer. Take 50 g of cinnamon powder, put it in a clean beaker, and soak it in 600 mL of ethanol and water composite solvent (ethanol volume fraction 65%) for 60 min. After soaking, adjust the pH of the solution to 5 with hydrochloric acid, put it into an ultrasonic instrument for ultrasonic extraction, 50 °C, 450 W, ultrasonic extraction for 40 min, filter under reduced pressure to separate the extract and cinnamon solid, and put the cinnamon solid in the original beaker again In the process, according to the solid-liquid ratio of 1:12g / mL, add ethanol-water composite solvent (ethanol volume fraction 65%), adjust the pH of the solution to 4 with hydrochloric acid, put it into an ultrasonic instrument for extraction, 50 ° C, 450 W, ultrasonic extraction After 40 min of extraction, filter under reduced pressure to separate the extract from the cinnamon solid, collect the extract, and disca...
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