Pyraoxystrobin pesticide preparation taking porous silicon dioxide as carrier and preparation method of pyraoxystrobin pesticide preparation
A technology of porous silica and mesoporous silica, applied in the field of pesticides, can solve problems such as poor transmission performance, achieve high drug loading rate, good transmission performance, and improve the effect of pesticide systemic absorption
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Embodiment 1
[0033]A pyraclostrobin pesticide preparation using porous silica as a carrier, the active ingredient is pyraclostrobin, the carrier is porous silica, the particle size of the porous silica is 200nm, and the porous silica is mesoporous Silica or microporous silica, the specific surface area of porous silica is 900.013m 2 / g, the pore diameter of porous silica is 1.487nm.
[0034] A preparation method of pyraclostrobin pesticide preparation using porous silicon dioxide as a carrier, dissolving all the pyraclostrobin original drug in an organic solvent, then adding porous silicon dioxide prepared by a sol-gel method, and fully mixing , centrifuged and dried to obtain pyraclostrobin pesticide preparation with porous silica as carrier.
[0035] Further, the mass ratio of pyraclostrobin to porous silica is 1:2, and the specific usage amounts are 15 mg of Pyr and 30 mg of MSN.
[0036] Further, the organic solvent is methanol.
[0037] Further, after adding porous silicon dioxid...
Embodiment 2
[0051] A pyraclostrobin pesticide preparation using porous silica as a carrier, the active ingredient is pyraclostrobin, the carrier is porous silica, the particle size of the porous silica is 100nm, and the porous silica is mesoporous Silica or microporous silica, the specific surface area of porous silica is 623.017m 2 / g, the pore diameter of porous silica is 2nm.
[0052] A preparation method of pyraclostrobin pesticide preparation using porous silicon dioxide as a carrier, dissolving all the pyraclostrobin original drug in an organic solvent, then adding porous silicon dioxide prepared by a sol-gel method, and fully mixing , centrifuged and dried to obtain pyraclostrobin pesticide preparation with porous silica as carrier.
[0053] Further, the mass ratio of pyraclostrobin to porous silica is 3:1, and the specific usage amounts are 90 mg of Pyr and 30 mg of MSN.
[0054] Further, the organic solvent is xylene.
[0055] Further, after adding porous silicon dioxide, st...
Embodiment 3
[0069] A pyraclostrobin pesticide preparation using porous silica as a carrier, the active ingredient is pyraclostrobin, the carrier is porous silica, the particle diameter of the porous silica is 15nm, and the porous silica is mesoporous Silica or microporous silica, the specific surface area of porous silica is 342.09m 2 / g, the pore diameter of porous silica is 2.743nm.
[0070] A preparation method of pyraclostrobin pesticide preparation using porous silicon dioxide as a carrier, dissolving all the pyraclostrobin original drug in an organic solvent, then adding porous silicon dioxide prepared by a sol-gel method, and fully mixing , centrifuged and dried to obtain pyraclostrobin pesticide preparation with porous silica as carrier.
[0071] Further, the mass ratio of pyraclostrobin to porous silica is 6:1, and the specific usage amounts are 180 mg of Pyr and 30 mg of MSN.
[0072] Further, the organic solvent is dichloromethane.
[0073] Further, after adding porous sil...
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