Secondary utilization method of inactivated non-noble metal vinyl chloride catalyst carrier
A catalyst carrier and non-precious metal technology, applied in chemical instruments and methods, applications, other chemical processes, etc., can solve the problems of short action time, inability to prevent the late decline of soil performance, and inability to maintain excellent soil performance for a long time, so as to achieve relief Storing and processing the effects of stress
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Embodiment 1
[0048] A method for secondary utilization of a deactivated non-noble metal vinyl chloride catalyst carrier, comprising: pretreatment, mixing, loading, immobilization activation, drying, mixing, and coating.
[0049] The pretreatment includes decompression impurity removal, acid treatment, rinse, microwave treatment, modification, drying and grinding.
[0050] For the impurity removal under reduced pressure, place the deactivated non-noble metal vinyl chloride catalyst under a vacuum degree of -0.07MPa, heat up to 150°C and keep warm for 2 hours; The precious metal vinyl chloride catalyst is shaken and mixed once; after the decompression and impurity removal is completed, the water content of the deactivated non-noble metal vinyl chloride catalyst is lower than 2%.
[0051] For the acid treatment, the deactivated non-precious metal vinyl chloride catalyst after decompression and impurity removal is put into 2 times the volume of the acid treatment solution, the temperature is r...
Embodiment 2
[0087] A method for secondary utilization of a deactivated non-noble metal vinyl chloride catalyst carrier, comprising: pretreatment, mixing, loading, immobilization activation, drying, mixing, and coating.
[0088] The pretreatment includes decompression impurity removal, acid treatment, rinse, microwave treatment, modification, drying and grinding.
[0089] For the impurity removal under reduced pressure, place the deactivated non-precious metal vinyl chloride catalyst under a vacuum degree of -0.09MPa, raise the temperature to 156°C and keep it for 2.5h; The non-noble metal vinyl chloride catalyst is shaken and mixed once; after the decompression and impurity removal is completed, the water content of the deactivated non-noble metal vinyl chloride catalyst is lower than 2%.
[0090] For the acid treatment, the deactivated non-precious metal vinyl chloride catalyst after decompression and impurity removal is put into 3 times the volume of the acid treatment solution, and the...
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