Compound herbicide containing dicamba and preparation method thereof
A dicamba and herbicide technology, applied in the field of pesticides, can solve the problems of limited herbicidal spectrum, complex process, long-lasting effect in the field, etc., to achieve the effect of improving the weeding effect, shortening the technological process, and avoiding residual toxicity
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Embodiment 1
[0033] Example 1: Herbicide containing 55% dicamba + 9.2% nicosulfuron + 2.3% rimsulfuron-methyl
[0034] The preparation method is as follows:
[0035] (1) Synthesis of dicamba sodium salt
[0036] Take 120 kg of dicamba technical and 35.2 kg of sodium carbonate, put them into a trough kneader, stir evenly, add 1.2 kg of water to continue kneading, leave it for about 60 minutes, and carry out rotary extrusion granulation.
[0037] Among them, the amount of sodium carbonate added is appropriately increased or decreased according to the change of the acidity of the original dicamba, and the pH of the sodium salt of dicamba is controlled between 7.0 and 9.0.
[0038] (2) Ingredients
[0039] Take the sample according to the following ingredient list:
[0040]
[0041] Accurately weigh the above materials (except dicamba sodium salt), mix well and set aside.
[0042] (3) Jet milling
[0043] The materials mixed in step (2) are pulverized in an airflow mill so that the fin...
Embodiment 2
[0048] Example 2: Herbicide containing 40% dicamba + 8% nicosulfuron + 2% rimsulfuron
[0049] The preparation method is as follows:
[0050] (1) Synthesis of dicamba sodium salt
[0051] Take 120 kg of dicamba technical and 35.2 kg of sodium carbonate, put them into a trough kneader, stir evenly, add 1.2 kg of water to continue kneading, leave it for about 60 minutes, and carry out rotary extrusion granulation.
[0052] Among them, the amount of sodium carbonate added is appropriately increased or decreased according to the change of the acidity of the original dicamba, and the pH of the sodium salt of dicamba is controlled between 7.0 and 9.0.
[0053] (2) Ingredients
[0054] Take the sample according to the following ingredient list:
[0055]
[0056] Accurately weigh the above materials (except dicamba sodium salt), mix well and set aside.
[0057] Other steps are identical with embodiment 1.
Embodiment 3
[0058] Embodiment 3: herbicide contains 60% dicamba+15% nicosulfuron
[0059] The preparation method is as follows:
[0060] (1) Synthesis of dicamba sodium salt
[0061] Take 120 kg of dicamba technical and 35.2 kg of sodium carbonate, put them into a trough kneader, stir evenly, add 1.2 kg of water to continue kneading, leave it for about 60 minutes, and carry out rotary extrusion granulation.
[0062] Among them, the amount of sodium carbonate added is appropriately increased or decreased according to the change of the acidity of the original dicamba, and the pH of the sodium salt of dicamba is controlled between 7.0 and 9.0.
[0063] (2) Ingredients
[0064] Take the sample according to the following ingredient list:
[0065]
[0066] Accurately weigh the above materials (except dicamba sodium salt), mix well and set aside.
[0067] Other steps are identical with embodiment 1.
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