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A kind of electroplated silver carbon fiber electrode and preparation method thereof

A carbon fiber electrode and silver electroplating technology, applied in the field of materials, can solve the problems of complex equipment, difficult to process carbon fiber continuously and stably for a long time, and achieve the effects of good potential range performance, low cost and good antibacterial properties

Active Publication Date: 2020-09-04
CHINA UNIV OF GEOSCIENCES (WUHAN)
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the generation of plasma requires a certain vacuum environment, and the required equipment is relatively complicated, which is difficult for continuous and stable carbon fiber processing and long-term processing.

Method used

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  • A kind of electroplated silver carbon fiber electrode and preparation method thereof
  • A kind of electroplated silver carbon fiber electrode and preparation method thereof
  • A kind of electroplated silver carbon fiber electrode and preparation method thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0020] The purity of raw materials used in the preparation method of the present invention are respectively AgNO 3 (>99.0%) (commercially available), NaNO 3 (>99.0%) (commercially available), carbon fiber (commercially available). According to the design formula of the electroplating solution, the required metering of raw materials is calculated according to the stoichiometric ratio.

[0021] refer to figure 1 , the preparation process of embodiment 1 is:

[0022] First weigh 2g of carbon fiber bundles and soak them in acetone solution for 24 hours to remove surface sizing agents and other impurities, then ultrasonically treat the carbon fiber bundles soaked in acetone solution for 30 minutes, and wash them with deionized water until neutral; then soak the carbon fiber bundles in ethanol solution And ultrasonic treatment for 30min, washed with deionized water until neutral, and then placed in a 60°C oven for 2h. Place the dried carbon fiber bundles in a muffle furnace for ...

Embodiment 2

[0027] The difference between Embodiment 2 and Embodiment 1 is only that the output voltage of the constant voltage power supply is 3V; the rest are basically the same as Embodiment 1.

Embodiment 3

[0029] The difference between embodiment 3 and embodiment 1 is only that the output voltage of the constant voltage power supply is 4V; the rest are basically the same as embodiment 1.

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Abstract

The invention provides a preparation method of an electroplated silver carbon fiber electrode. The preparation method comprises the following steps of weighing carbon fiber bundle and soaking the carbon fiber bundle in an acetone solution, then performing ultrasonic treatment, and soaking the carbon fiber bundle in an ethanol solution for ultrasonic treatment; placing the carbon fiber bundle in amuffle furnace for thermal oxidation treatment, then performing ultrasonic cleaning with deionized water, and then placing in a drying oven for drying; cutting the carbon fiber bundle subjected to oxidation treatment to a certain length, and binding one end of the cut carbon fiber bundle with a silver wire for fixation; mixing AgNO<3> and NaNO<3> solution to prepare electroplating solution, placing a pair of carbon fiber bundles in the electroplating solution, supplying voltage by a constant-voltage power supply, electroplating the carbon fiber bundles to obtain silver-plated carbon fibers, and packaging the silver-plated carbon fibers in a heat-shrinkable tube to obtain the silver-plated carbon fiber electrode. The preparation method is simple; and the electroplated silver carbon fiber electrode prepared by the method has small range, stable performance, and easy long-term storage and can be used for detecting ocean electric field signals.

Description

technical field [0001] The invention relates to the technical field of materials, in particular to a silver-plated carbon fiber electrode and a preparation method thereof. Background technique [0002] Carbon fiber has the advantages of large specific surface area and good chemical stability in the marine environment, and is suitable as a marine electric field sensor. In the 1970s, the U.S. Naval Postgraduate School conducted research on different electrode materials as sensors for detecting ocean electric fields. The report pointed out that Ag / AgCl electrodes, Pt / Pt black electrodes and carbon fiber electrodes have low impedance, and these materials are suitable for use as ocean electrodes. Among them, carbon fiber electrodes have the lowest cost and are suitable for large-scale use. In 2003, at the European Underwater Defense Technology (UDT) conference, the Swedish Polyamp company demonstrated a self-developed carbon fiber sensor for detecting underwater electric fields ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C25D7/06C25D5/54C25D3/46D01D10/02G01R29/12
CPCC25D3/46C25D5/54C25D7/0607D01D10/02G01R29/12
Inventor 徐建梅胡智慧黄灿何天成李文昊
Owner CHINA UNIV OF GEOSCIENCES (WUHAN)
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