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Preparation method of adsorbent for wastewater treatment

A wastewater treatment and adsorbent technology, which is applied in textile industry wastewater treatment, adsorption water/sewage treatment, oxidized water/sewage treatment, etc., can solve the problems of inability to degrade organic pollutants, poor removal effect of dye wastewater, single effect of adsorbent, etc. problems, to achieve good biocompatibility, high water retention, inhibition of recombination

Inactive Publication Date: 2019-05-17
南京思宇环保科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

This patented technology relates to a new type of chemical called strontum carbonate (SCO) that helps break down harmful substances into smaller particles more efficiently than traditional methods like adding iron or aluminum oxides alone. It was found effective at reducing various types of contaminations such as pesticides, metals, dyes, explosives, nitrogen compounds, pharmaceutical agents, and other materials.

Problems solved by technology

This patented describes different types of materials called dyers' detergents (DDS) such as quaternary ammonium salt compounds like DYELLOX®, DOCARBOXYLONES™, polyoxyethylene diamine polymer(PED), polysilane resin, carboxymethylethanes, chlorophyll salts, cyanobacteria algae, and others. These substances have negative impact on human health because their presence affects the environment negatively while causing damage to aquatic ecosystems. Existing techniques involve expensive and time-consuming processes involving complicated steps and disposable products made up mostly of synthetic agents.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

example 1

[0030] Preparation of alkalized deacetylated flocculant:

[0031] Mix fly ash, lapis lazuli, and coke in a mass ratio of 10:4:1, place in a muffle furnace, heat up to 400°C, and roast for 3 hours to obtain high-temperature activated powder. In parts by weight, 20 parts of high-temperature Put activating powder and 4 parts of mixed carbonizing agent into 80 parts of hot water at 60°C, wherein the mixed carbonizing agent is prepared by mixing ammonium bicarbonate and strontium hydroxide octahydrate at a mass ratio of 5:1, and let it stand for 2 hours after stirring , remove the upper layer, and collect the lower sediment;

[0032] Mix the above-mentioned lower sediment, phenol, furfural, and sodium carbonate in a mass ratio of 7:8:10:1 and put them into a reaction kettle, heat up to 50°C, keep warm for 10 hours to obtain phenolic gel, and age for 10 hours to obtain The gel doped with strontium carbonate was placed in dry ice and freeze-dried for 2 hours to obtain airgel. The ai...

example 2

[0040] Preparation of alkalized deacetylated flocculant:

[0041] Mix fly ash, lapis lazuli, and coke in a mass ratio of 10:4:1, place in a muffle furnace, heat up to 450°C, and roast for 3.5 hours to obtain high-temperature activated powder. In parts by weight, 20- Put 30 parts of high-temperature activation powder and 4 parts of mixed carbonizing agent into 90 parts of hot water at 80°C, wherein the mixed carbonizing agent is prepared by mixing ammonium bicarbonate and strontium hydroxide octahydrate at a mass ratio of 5:1. After stirring Stand still for 2.5 hours, remove the upper layer, and collect the lower layer of sediment;

[0042] Mix the above-mentioned lower sediment, phenol, furfural, and sodium carbonate in a mass ratio of 7:8:10:1 and put them into a reaction kettle, heat up to 52°C, and keep warm for 11 hours to obtain a phenolic gel, which is aged for 11 hours to obtain The gel doped with strontium carbonate was placed in dry ice and freeze-dried for 2.5 hours...

example 3

[0050] Preparation of alkalized deacetylated flocculant:

[0051] Mix fly ash, lapis lazuli, and coke in a mass ratio of 10:4:1, place in a muffle furnace, heat up to 500°C, and roast for 4 hours to obtain high-temperature activated powder. In parts by weight, 30 parts of high-temperature Put activating powder and 5 parts of mixed carbonizing agent into 100 parts of hot water at 100°C, wherein the mixed carbonizing agent is prepared by mixing ammonium bicarbonate and strontium hydroxide octahydrate at a mass ratio of 5:1, and let it stand for 3 hours after stirring , remove the upper layer, and collect the lower sediment;

[0052] Mix the above-mentioned lower sediment, phenol, furfural, and sodium carbonate in a mass ratio of 7:8:10:1 and put them into a reaction kettle, heat up to 55°C, keep warm for 12 hours to obtain a phenolic gel, and age for 12 hours to obtain The gel doped with strontium carbonate was then placed in dry ice and freeze-dried for 3 hours to obtain airge...

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PUM

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Abstract

The invention discloses a preparation method of an adsorbent for wastewater treatment, and belongs to the technical field of wastewater treatment. According to the preparation method, fly ash is subjected to acid leaching treatment, the adsorption capability of the fly ash to dye can be significantly enhanced, chitosan is adopted to be composited with the fly ash, the fly ash is adsorbed on the surface of the chitosan in the compositing process, the electrical property of the surface of the fly ash is changed, dye wastewater is generally negatively charged, in this way, the fly ash has the surface adsorption capability, the treatment effect of wastewater is enhanced, strontium carbonate extracted from celestite is doped in the fly ash, the strontium carbonate can make titanium dioxide lattices distorted, thus an energy gap of a titanium dioxide forbidden band is narrowed, titanium dioxide can absorb light with the wider-scope wavelength, a culture matrix containing bacillus natto liquid is prepared from soybean powder and is rich in gamma-polyglutamic acid, the space reserved after the gamma-polyglutamic acid is biodegraded provides the space for subsequent microorganism growth, the number of the active microorganisms on the adsorbent is increased, and thus the biofilm culturing amount of the adsorbent microorganisms is increased.

Description

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Claims

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Application Information

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Owner 南京思宇环保科技有限公司
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