Preparation method of adsorbent for wastewater treatment
A wastewater treatment and adsorbent technology, which is applied in textile industry wastewater treatment, adsorption water/sewage treatment, oxidized water/sewage treatment, etc., can solve the problems of inability to degrade organic pollutants, poor removal effect of dye wastewater, single effect of adsorbent, etc. problems, to achieve good biocompatibility, high water retention, inhibition of recombination
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example 1
[0030] Preparation of alkalized deacetylated flocculant:
[0031] Mix fly ash, lapis lazuli, and coke in a mass ratio of 10:4:1, place in a muffle furnace, heat up to 400°C, and roast for 3 hours to obtain high-temperature activated powder. In parts by weight, 20 parts of high-temperature Put activating powder and 4 parts of mixed carbonizing agent into 80 parts of hot water at 60°C, wherein the mixed carbonizing agent is prepared by mixing ammonium bicarbonate and strontium hydroxide octahydrate at a mass ratio of 5:1, and let it stand for 2 hours after stirring , remove the upper layer, and collect the lower sediment;
[0032] Mix the above-mentioned lower sediment, phenol, furfural, and sodium carbonate in a mass ratio of 7:8:10:1 and put them into a reaction kettle, heat up to 50°C, keep warm for 10 hours to obtain phenolic gel, and age for 10 hours to obtain The gel doped with strontium carbonate was placed in dry ice and freeze-dried for 2 hours to obtain airgel. The ai...
example 2
[0040] Preparation of alkalized deacetylated flocculant:
[0041] Mix fly ash, lapis lazuli, and coke in a mass ratio of 10:4:1, place in a muffle furnace, heat up to 450°C, and roast for 3.5 hours to obtain high-temperature activated powder. In parts by weight, 20- Put 30 parts of high-temperature activation powder and 4 parts of mixed carbonizing agent into 90 parts of hot water at 80°C, wherein the mixed carbonizing agent is prepared by mixing ammonium bicarbonate and strontium hydroxide octahydrate at a mass ratio of 5:1. After stirring Stand still for 2.5 hours, remove the upper layer, and collect the lower layer of sediment;
[0042] Mix the above-mentioned lower sediment, phenol, furfural, and sodium carbonate in a mass ratio of 7:8:10:1 and put them into a reaction kettle, heat up to 52°C, and keep warm for 11 hours to obtain a phenolic gel, which is aged for 11 hours to obtain The gel doped with strontium carbonate was placed in dry ice and freeze-dried for 2.5 hours...
example 3
[0050] Preparation of alkalized deacetylated flocculant:
[0051] Mix fly ash, lapis lazuli, and coke in a mass ratio of 10:4:1, place in a muffle furnace, heat up to 500°C, and roast for 4 hours to obtain high-temperature activated powder. In parts by weight, 30 parts of high-temperature Put activating powder and 5 parts of mixed carbonizing agent into 100 parts of hot water at 100°C, wherein the mixed carbonizing agent is prepared by mixing ammonium bicarbonate and strontium hydroxide octahydrate at a mass ratio of 5:1, and let it stand for 3 hours after stirring , remove the upper layer, and collect the lower sediment;
[0052] Mix the above-mentioned lower sediment, phenol, furfural, and sodium carbonate in a mass ratio of 7:8:10:1 and put them into a reaction kettle, heat up to 55°C, keep warm for 12 hours to obtain a phenolic gel, and age for 12 hours to obtain The gel doped with strontium carbonate was then placed in dry ice and freeze-dried for 3 hours to obtain airge...
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