Organic Compounds and Organic Electroluminescent Devices
A compound and organic layer technology, applied in organic chemistry, electro-solid devices, light-emitting materials, etc., can solve the problems of device efficiency and lifespan, and achieve the effect of strong electricity richness, lower sublimation temperature, and adjustment of transmission performance.
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[0102] In order to enable those skilled in the art to better understand the present invention, the present invention will be further described in detail below in conjunction with specific embodiments.
[0103] Synthetic example
[0104] The compounds of the present invention can be synthesized from commercially available starting materials by conventional reaction steps. Representative synthetic routes such as:
[0105] Synthetic route G1:
[0106]
[0107] Synthetic route G2:
[0108]
[0109] The specific synthetic method of individual representative compound of the present invention is given below:
[0110]
[0111] Add pd (dppf )cl 2 (0.86g, 1.18mmol) and SPhos (0.97g, 2.36mmol). The resulting reaction mixture was heated to 90 C under nitrogen atmosphere and stirred overnight. After the reaction solution was cooled to room temperature, it was diluted with toluene and washed with water. After separation, the organic phase was dried over MgSO4. After the s...
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