Multi-stage pressurized fluorination treatment method of surface of plastic part
A technology for fluorination treatment and plastic parts, which is applied in the field of multi-stage pressurized fluorination treatment on the surface of plastic parts, which can solve the problems of surface modification and recovery, surface energy decline, etc. stable effect
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Embodiment 1
[0041] Embodiment 1: The surface treatment method for plastic parts consists of the following steps:
[0042] 1) Clean and dry the plastic parts;
[0043] 2) Put the dried plastic parts into the airtight reaction chamber of the fluorination equipment, feed nitrogen gas, and replace the air in the reaction chamber 4 times;
[0044] 3) Preheat the internal temperature of the reaction chamber to 40°C, and then pass a mixed gas of fluorine, nitrogen and oxygen to react. The volume ratio of fluorine and nitrogen in the mixed gas is 1:9, and the volume ratio of oxygen It is 1 / 400 of the volume of fluorine gas; the reaction is divided into the following five pressure stages:
[0045] In the first pressure stage, the internal pressure of the reaction chamber is adjusted to 5mbar;
[0046] In the second pressure stage, the internal pressure of the reaction chamber is adjusted to 20mbar;
[0047] In the third pressure stage, the internal pressure of the reaction chamber is adjusted t...
Embodiment 2
[0062] Embodiment 2: The surface treatment method for plastic parts consists of the following steps:
[0063] 1) Clean and dry the plastic parts;
[0064] 2) Put the dried plastic parts into the airtight reaction chamber of the fluorination equipment, feed nitrogen gas, and replace the air in the reaction chamber 4 times;
[0065] 3) Preheat the internal temperature of the reaction chamber to 40°C, and then pass a mixed gas of fluorine, nitrogen and oxygen to react. The volume ratio of fluorine and nitrogen in the mixed gas is 1:9, and the volume ratio of oxygen It is 1 / 400 of the volume of fluorine gas; the reaction is divided into the following five pressure stages:
[0066] In the first pressure stage, the internal pressure of the reaction chamber is adjusted to 8mbar;
[0067] In the second pressure stage, the internal pressure of the reaction chamber is adjusted to 15mbar;
[0068] In the third pressure stage, the internal pressure of the reaction chamber is adjusted t...
Embodiment 3
[0076] Embodiment 3: The surface treatment method for plastic parts consists of the following steps:
[0077] 1) Clean and dry the plastic parts;
[0078] 2) Put the dried plastic parts into the airtight reaction chamber of the fluorination equipment, feed nitrogen gas, and replace the air in the reaction chamber for 5 times;
[0079] 3) Preheat the internal temperature of the reaction chamber to 45°C, and then pass a mixed gas of fluorine, nitrogen and oxygen to react. The volume ratio of fluorine and nitrogen in the mixed gas is 1:8, and the volume ratio of oxygen It is 1 / 300 of the volume of fluorine gas; the reaction is divided into the following 4 pressure stages:
[0080] In the first pressure stage, the internal pressure of the reaction chamber is adjusted to 10mbar;
[0081] In the second pressure stage, the internal pressure of the reaction chamber is adjusted to 30mbar;
[0082] In the third pressure stage, the internal pressure of the reaction chamber is adjusted...
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