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Method for determining volatile components of tobacco blasting bead by solid phase microextraction-gas chromatography-mass spectrometry

A volatile component, solid-phase micro-extraction head technology, applied in the field of tobacco, to achieve good separation effect

Active Publication Date: 2018-09-18
CHINA TOBACCO SHAANXI IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] At present, there have been many cigarettes characterized by built-in "popping beads" at home and abroad, and some cigarette products have been gradually developed, but the determination of the volatile components in the "popping beads" by solid phase The method has not been reported

Method used

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  • Method for determining volatile components of tobacco blasting bead by solid phase microextraction-gas chromatography-mass spectrometry
  • Method for determining volatile components of tobacco blasting bead by solid phase microextraction-gas chromatography-mass spectrometry
  • Method for determining volatile components of tobacco blasting bead by solid phase microextraction-gas chromatography-mass spectrometry

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] 1 Samples, standards and instruments

[0030] 1.1 Instruments and equipment

[0031] GC-MS Gas Chromatography-Mass Spectrometry Instrument US PE Company; Supelco Solid Phase Microextraction Device US Supelco Company; Extraction head is 65 μm PDMS / DVB extraction head US Supelco Company.

[0032] 1.2 Sample

[0033] Randomly select cigarette products containing explosive beads from China Tobacco Industry Co., Ltd. in Shaanxi Province.

[0034] 2. Adsorption and desorption of aroma substances

[0035] Put the solid-phase micro-extraction head in the gas chromatograph inlet and age it at 250°C for 30 minutes for standby; randomly select 20 cigarettes, take out the cigarette popping beads and put them into the solid-phase micro-extraction bottle, quickly break the popping beads and seal them with the lid . Put it in a constant temperature water bath at 80°C for 30 minutes to fully volatilize and balance the aroma; then insert the needle of the solid phase microextraction...

Embodiment 2

[0047] 1. Comparison of different extraction methods

[0048] Method 1: Randomly select 20 pop-up beads, break the pop-up beads, add 20mL dichloromethane for ultrasonic extraction for 30min, take out the sample and let it stand for 30min, filter it through a 0.45μm organic phase needle filter membrane, and then perform GC-MS detection; the spectrum of the sample is as follows: image 3 and shown in Table 2.

[0049] Table 2 Dichloromethane Ultrasonic Extraction Component Analysis Table

[0050] serial number

keep time

name

CAS number

molecular formula

1

4.56

Dihydrofuran

1191-99-7

C 4 h 6 o

2

6.86

L-menthol

2216-51-5

C10H20O

3

36.67

Glyceryl Tricaprylate

538-23-8

C27H50O6

4

37.009

Glyceryl Tricaprylate Isomers

538-23-8

C27H50O6

5

44.42

Glyceryl tricaprate

621-71-6

C33H62O6

6

48.02

Glyceryl Tricaprylate Isomers

538-23-8

C27H50O6

...

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Abstract

chromatography-mass spectrometry, the method comprises the following steps: 1) placing the blasting bead into a solid phase micro-extraction bottle, crushing, covering the solid phase micro-extractionbottle with a solid phase micro-extraction bottle cap, then heating to volatilize and balance components in the blasting bead; aging a solid phase micro-extraction head; 2) inserting the solid phasemicro-extraction head into the solid phase micro-extraction bottle, and adsorbing at 40-120 DEG C for 60-240 min; 3) inserting the adsorbed solid phase micro-extraction head into a sample inlet of a GC-MS instrument, and thermally desorbing at 230-280 DEG C for 1-2 min; and 4) running the GC-MS instrument and collecting data. The method can conveniently, quickly and accurately analyze the volatilecomponents in the blasting bead and avoids the interference and pollution caused by a solvent in the blasting bead. The peak type has no tailing phenomenon, and the components are separated. The components basically cover the common components of the blasting bead, and the method has a good separation and detection effect, and provides an analytical basis for the research and development of a newblasting bead, quality control of blasting bead production, component analysis of blasting bead products, and the like.

Description

technical field [0001] The invention belongs to the technical field of tobacco, and in particular relates to a method for determining the volatile components of popping beads for cigarettes by solid-phase microextraction-gas chromatography. Background technique [0002] In recent years, the appearance of "popping beads" filter sticks has made the methods of tobacco flavoring more diversified, and the use of some extremely volatile and unstable flavors and fragrances and functional additives has also become possible. The functions of "Bangzhu" in supplementing, improving and coordinating the quality of cigarette smoking and improving, changing, and the style of cigarette products are becoming more and more prominent. Consumers welcome. [0003] The so-called Breakable Capsules, also known as incense pills, brittle capsules, and beads, have a diameter of 26-35 μm and a weight of about 0.020 g. They refer to beads that can be squeezed. It is used in sticks and to a lesser ext...

Claims

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Application Information

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IPC IPC(8): G01N30/02G01N30/06
CPCG01N30/02G01N30/06G01N2030/062
Inventor 王瑶彭军仓樊亚玲吕娟康世平张萌萌孙赵麟张凤侠
Owner CHINA TOBACCO SHAANXI IND
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