A kind of denture hydrogel spacer material and preparation method thereof
A hydrogel and spacer technology, which is applied in pharmaceutical formulations, dental preparations, tooth protection coatings, etc., can solve the problems of denture spacers with single function, periodontal swelling, bleeding, and gingivitis, and achieve a bactericidal effect The effect of improving, improving chewing efficiency, and improving aesthetics
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Embodiment 1
[0018] A denture hydrogel spacer material is made of the following raw materials in parts by weight:
[0019] Palm fiber 5, sodium hypochlorite 3, peppermint oil 4, longan core 2, nettle root 3, chitosan 30, polyvinyl alcohol solution 50, glutaraldehyde solution 15;
[0020] The mass fraction of the glutaraldehyde solution is 30%.
[0021] Further, the preparation method of the polyvinyl alcohol solution is as follows: adding polyvinyl alcohol into deionized water 5 times its volume, heating to 40°C to fully dissolve it, then adding tea tree oil, stirring evenly, and placing it in a water bath at 70°C , stirred and swelled for 3h, then raised the temperature to 80°C and stirred for 20min.
[0022] Further, its preparation method comprises the following steps:
[0023] (1) Put the palm fiber into a pulverizer for 10 minutes, pass through a 200-mesh sieve, immerse in distilled water 15 times the volume of the palm fiber, heat and stir until boiling, let it fully swell for 20 m...
Embodiment 2
[0029] A denture hydrogel spacer material is made of the following raw materials in parts by weight:
[0030] Palm fiber 6, sodium hypochlorite 4, peppermint oil 5, longan core 3, nettle root 4, chitosan 40, polyvinyl alcohol solution 60, glutaraldehyde solution 17;
[0031] The mass fraction of the glutaraldehyde solution is 40%.
[0032] Further, the preparation method of the polyvinyl alcohol solution is as follows: adding polyvinyl alcohol into deionized water 7 times its volume, heating to 45°C to fully dissolve it, then adding tea tree oil, stirring evenly, and placing it in a water bath at 72°C , stirred and swelled for 3.5 hours, then raised the temperature to 82°C and stirred for 25 minutes.
[0033] Further, its preparation method comprises the following steps:
[0034] (1) Put the palm fiber into a pulverizer for 15 minutes, pass through a 250-mesh sieve, immerse in distilled water 17 times the volume of the palm fiber, heat and stir until it boils, make it fully ...
Embodiment 3
[0040]A denture hydrogel spacer material is made of the following raw materials in parts by weight:
[0041] Palm fiber 10, sodium hypochlorite 5, peppermint oil 6, longan core 5, nettle root 6, chitosan 50, polyvinyl alcohol solution 80, glutaraldehyde solution 20;
[0042] The mass fraction of the glutaraldehyde solution is 50%.
[0043] Further, the preparation method of the polyvinyl alcohol solution is as follows: adding polyvinyl alcohol into deionized water 10 times its volume, heating to 50°C to fully dissolve it, then adding tea tree oil, stirring evenly, and placing it in a water bath at 75°C , stirred and swelled for 4h, then raised the temperature to 85°C and stirred for 30min.
[0044] Further, its preparation method comprises the following steps:
[0045] (1) Put the palm fiber into a pulverizer for 20 minutes, pass through a 300-mesh sieve, immerse in distilled water 20 times the volume of the palm fiber, heat and stir until boiling, make it fully swell for 30...
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