A multi-stage liquefaction process of coal and biomass
A biomass and process technology, applied in the field of coal and biomass co-refining process, can solve the problems of low liquefaction efficiency, limited coal powder content, and no realization of coal, biomass and oil mixing production technology and other problems
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Embodiment 1
[0087] A multi-stage liquefaction process of coal and biomass, comprising the following steps:
[0088] (1) Take lignite, dry and dehydrate it, pulverize to a median particle size of 50 μm, and then send it to a briquetting machine for extrusion molding at a molding pressure of 5 MPa to obtain lignite compressed material. The compressed lignite material is sent to a hammer mill for pulverization to obtain a pulverized lignite material with a particle size of 30 μm. The above-mentioned pulverized lignite material and the amorphous ferric oxyhydroxide after sulfidation treatment in the reactor are added to the mixture of liquid manure and waste oil to form a biomass kerosene slurry, and hydrogen gas is passed into the biomass kerosene slurry to generate One-stage hydrogenation reaction to obtain one-stage hydrogenation product.
[0089] (2) Then add the amorphous alumina loaded with Mo oxide and Ni oxide sulfurized in the reactor to the primary hydrogenation product and feed hy...
Embodiment 2
[0091] A multi-stage liquefaction process of coal and biomass, comprising the following steps:
[0092] Straw pretreatment:
[0093] Take wheat stalks and corn stalks, dry and dehydrate them, crush them to a median particle size of 100 μm, and then send them to a layering machine for extrusion molding at a molding pressure of 2 MPa to obtain straw compressed materials;
[0094] Send the straw compressed material into a hammer mill for crushing to obtain a straw crushed material with a median particle size of 30 μm, which is ready for use.
[0095] Pretreatment of coal raw materials:
[0096] Take lignite, dry and dehydrate it, pulverize until the median particle size is 100 μm, and then send it into a briquetting machine for extrusion molding, and the molding pressure is 15MPa to obtain lignite compressed material;
[0097] Send the compressed lignite material into a ball mill for pulverization to obtain a pulverized lignite material with a median particle size of 50 μm, ...
Embodiment 3
[0111] A multi-stage liquefaction process of coal and biomass, comprising the following steps:
[0112] Pretreatment of biomass raw materials:
[0113] (1) Get the reed, dry and dehydrate it, and then send it to the jet mill for crushing to obtain the primary crushed material of the reed, with a particle size of D 50 is 300 μm.
[0114] (2) Send the reed primary pulverized material into a briquetting machine or a plodder for extrusion molding with a molding pressure of 5 MPa to obtain a reed compressed material.
[0115] (3) The reed compressed material is sent into the jet mill, and secondary pulverization is carried out to obtain the reed secondary pulverization material, particle size D 50 50 μm, ready for use.
[0116] Pretreatment of coal raw materials:
[0117] (1) Take Shendong long-flame coal, dry and dehydrate it, and then send it to a ball mill for crushing to obtain primary crushed material of Shendong long-flame coal, particle size D 50 is 80 μm.
[0118]...
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