Preparation method of adsorption material for organic pollutants in atmosphere

A technology for organic pollutants and adsorption materials, which is applied in the field of preparation of adsorbent materials, can solve the problems of reducing hygroscopicity, easy to absorb water vapor, reducing and other problems, and achieve the effect of improving adsorption effect, simple process, low-cost large-scale production

Inactive Publication Date: 2017-09-22
CHANGZHOU TANXING TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

For VOC in the air, the commonly used adsorption materials on the market are activated carbon or activated carbon fiber, but they all have the disadvantage of being easy to absorb water vapor, especially in coastal areas with high humidity and more serious moisture absorption, so that the effective adsorption space will be occupied and used The space for adsorbing pollutants is reduced
The existing activated carbon contains a large number of hydrophilic functional groups, which is the reason for its hygroscopicity, but at the same time, these functional groups are effective adsorption sites for adsorbing pollutant gases, so the hygroscopicity cannot be reduced by removing functional groups

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] A preparation method for an adsorption material for organic pollutants in the atmosphere, comprising the following steps:

[0024] Ultrasonic disperse 50g of graphene oxide in water to obtain a graphene oxide dispersion; control the concentration of the graphene oxide dispersion to 0.1mg / ml, add hydrazine hydrate containing 7g of hydrazine to the graphene oxide dispersion, and stir for 2min; 50g of activated carbon was immersed in the graphene oxide dispersion, and sealed; the mixture was heated to 85°C, kept for 24h, and dried to obtain the product. Wherein, activated carbon is any commercially available activated carbon.

Embodiment 2

[0026] A preparation method for an adsorption material for organic pollutants in the atmosphere, comprising the following steps:

[0027] Ultrasonically disperse 100g of graphene oxide in water to obtain a graphene oxide dispersion; control the concentration of the graphene oxide dispersion to 5mg / ml, add 100g of vitamin C to the graphene oxide dispersion, and stir for 5min; immerse 50g of activated carbon in the oxidation In the graphene dispersion liquid, seal; heat the mixture to 95°C, keep it for 0.5h, and dry to obtain the product. Wherein, activated carbon is any commercially available activated carbon.

Embodiment 3

[0029] A preparation method for an adsorption material for organic pollutants in the atmosphere, comprising the following steps:

[0030] Ultrasonically disperse 100g of graphene oxide in water to obtain a graphene oxide dispersion; control the concentration of the graphene oxide dispersion to 2mg / ml, add 100g of vitamin C to the graphene oxide dispersion, and stir for 3min; immerse 50g of activated carbon in the oxidation In the graphene dispersion, seal; heat the mixture to 90°C, keep it for 12h, and dry to obtain the product. Wherein, activated carbon is any commercially available activated carbon.

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Abstract

The invention relates to the field of new materials and environmental protection, in particular to a preparation method of an adsorption material for organic pollutants in the atmosphere. The method includes the following steps that a graphene oxide dispersion is prepared; a reducing agent is added into the graphene oxide dispersion, and stirring is conducted for 2-5 min; activated carbon is soaked in the graphene oxide dispersion and sealed; the mixture is heated to 85-95 DEG C and the temperature is kept for 0.5-24 hours, and the product is obtained after drying. According to the method, the hydrophobicity of graphene can be effectively used for preventing the adsorption of water vapor, at the same time, the gaseous organic pollutant adsorption of active sites of activated carbon is not affected, and the adsorption effect of activated carbon is significantly improved. In addition, the process is simple and the low-cost large-scale production can be achieved.

Description

technical field [0001] The invention relates to the fields of new materials and environmental protection, in particular to a method for preparing an adsorption material for organic pollutants in the atmosphere. Background technique [0002] With the development of industry, a large amount of volatile organic pollutants (VOC) escape into the atmosphere, causing serious air pollution. For VOC in the air, the commonly used adsorption materials on the market are activated carbon or activated carbon fiber, but they all have the disadvantage of being easy to absorb water vapor, especially in coastal areas with high humidity and more serious moisture absorption, so that the effective adsorption space will be occupied and used The space for adsorbing pollutants is reduced. The existing activated carbon contains a large number of hydrophilic functional groups, which is the reason for its hygroscopicity, but at the same time, these functional groups are effective adsorption sites for...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J20/20B01J20/32B01D53/02
CPCB01D53/02B01D2257/708B01D2258/06B01J20/20B01J20/3204B01J20/324B01J2220/4806
Inventor 毕恒昌
Owner CHANGZHOU TANXING TECH CO LTD
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