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A kind of desalination method of producing l-alanine feed liquid by fermentation method

A technology of alanine and fermentation method, applied in the direction of organic chemistry method, chemical instrument and method, preparation of organic compounds, etc., can solve the problems affecting the quality of L-alanine, and achieve the effect of quality assurance

Active Publication Date: 2019-04-02
QINHUANGDAO HUAHENG BIOENG CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

High salt content such as phosphate and ammonium salt seriously affects the quality of L-alanine finished product

Method used

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  • A kind of desalination method of producing l-alanine feed liquid by fermentation method
  • A kind of desalination method of producing l-alanine feed liquid by fermentation method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0033] The phosphate content in the feed liquid to be treated is 4260ppm, and the ammonium salt content is 6573ppm. Use caustic soda to adjust its pH value to 8.5, add 0.06% magnesium oxide, stir and mix. The rotation speed of the vacuum drum is 1.5r / min, and the vacuum degree is 0.03-0.08MPa. After salt precipitation, vacuum drum filtration, evaporation crystallization and other processes, the phosphate content in the resulting finished product is 153ppm, and the ammonium salt content is 84ppm. Compared with the original process, the removal rate of phosphate is increased by about 76.5%, and the removal rate of ammonium salt is increased by 79%.

Embodiment 2

[0035] The phosphate content in the feed liquid to be treated is 3763ppm, and the ammonium salt content is 5941ppm. Use caustic soda to adjust its pH value to 8.5, add 0.08% calcium oxide, stir and mix. The rotation speed of the vacuum drum is 1.5r / min, and the vacuum degree is 0.03-0.08MPa. After salt precipitation, vacuum drum filtration, evaporation crystallization and other processes, the phosphate content in the resulting finished product is 182ppm, and the ammonium salt content is 106ppm. Compared with the original process, the removal rate of phosphate is increased by about 73.5%, and the removal rate of ammonium salt is increased by 77.2%.

Embodiment 3

[0037] The phosphate content in the feed liquid to be treated is 5794ppm, and the ammonium salt content is 7201ppm. Use caustic soda to adjust its pH value to 7.5, add 0.08% magnesium oxide, stir and mix. The rotation speed of the vacuum drum is 1.5r / min, and the vacuum degree is 0.03-0.08MPa. After salt precipitation, vacuum drum filtration, evaporation crystallization and other processes, the phosphate content in the resulting finished product is 173ppm, and the ammonium salt content is 113ppm. Compared with the original process, the removal rate of phosphate is increased by about 73.4%, and the removal rate of ammonium salt is increased by 71.7%.

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Abstract

A desalting method for an L-alanine material liquid produced by a fermentation process is disclosed. The method mainly includes salt precipitation, vacuum rotary drum filtering, and other types of operation. A fermentation material liquid of L-alanine produced by the fermentation process has high salt contents and complex components. In the method, after a material liquid to be treated is subjected to salt precipitation, vacuum rotary drum filtering, and other types of operation, contents of ammonium salts, phosphates, and other components in an obtained product are reduced by 70% or above than those in an original process, and can be stably controlled in a qualified range, thus achieving an objective of effectively removing salts.

Description

technical field [0001] The invention relates to the production field of L-alanine, in particular to a method for effectively desalting the fermentation feed liquid of L-alanine produced by the fermentation method, and comprehensively utilizing processes such as salt precipitation and vacuum drum filtration to achieve the purpose of desalting . Background technique [0002] In the traditional amino acid extraction process, the feed liquid to be treated is directly poured into the centrifuge after being evaporated and crystallized, and then centrifuged to discharge the material to obtain the product, such as figure 1 shown. There is no specific desalination operation in the traditional process, which often results in high salt content in the product, and it is difficult to meet the qualified standard for the salt content of the product. [0003] The fermentation method is adopted to produce L-alanine, the phosphate content in the feed liquid to be treated is 1000-6000ppm, an...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C07C229/08C07C227/40
CPCC07B2200/07C07C227/40C07C229/08
Inventor 刘洋唐思青张冬竹
Owner QINHUANGDAO HUAHENG BIOENG CO LTD
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