Lubricating oil extreme pressure agent and preparation method thereof
A technology of extreme pressure agent and lubricating oil, which is applied in the direction of lubricating compositions, additives, petroleum industry, etc., can solve the problems of poor extreme pressure performance and high production cost, and achieve good extreme pressure performance, low production cost and good production requirements Effect
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Embodiment 1
[0018] Example 1, the lubricating oil extreme pressure agent is obtained according to the following preparation method: the first step, adding concentrated sulfuric acid to vegetable oil for reaction, and the first mixed liquid is obtained after the reaction; the second step, adding alkali or lye to adjust the first The pH value of the mixed solution is adjusted to obtain the second mixed solution; in the third step, the second mixed solution is dehydrated to obtain a lubricating oil extreme pressure agent. The lye can be saturated lye.
Embodiment 2
[0019] Embodiment 2, as the optimization of above-mentioned embodiment, in the first step, the add-on of concentrated sulfuric acid is 5% to 10% of vegetable oil quality; Or / and, in the first step, concentrated sulfuric acid joins in vegetable oil, at temperature React at 20°C to 60°C for 50min to 90min; or / and, in the first step, the concentrated sulfuric acid and vegetable oil are reacted under stirring, and the stirring rate is 60rpm to 100rpm.
Embodiment 3
[0020] Example 3, as an optimization of the above example, in the second step, add alkali or lye to adjust the pH value of the first mixed solution to 7 to 8; or / and, in the second step, the alkali is sodium hydroxide or hydroxide Calcium; lye is sodium hydroxide aqueous solution or calcium hydroxide aqueous solution.
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