Transparent rose toilet soap and preparation method thereof
A technology for transparent soap and roses, which is applied in chemical instruments and methods, soap detergents and other compounding agents, alkali soap/ammonium soap compositions, etc., can solve the problems of high irritation, complex components, and limited application scope.
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Embodiment 1
[0042] A method for preparing rose transparent soap, comprising steps:
[0043] 1) Add 8 parts by weight of oil into the jacketed pot, heat and melt the oil, and control the oil temperature to 80-85°C;
[0044] 2) dissolving 0.02 parts by weight of EDTA and 0.9 parts by weight of caustic soda with 2.08 parts by weight of rose distilled water, and preparing 3 parts by weight of 30% NaOH solution;
[0045] 3) Slowly add the 30% NaOH solution prepared in the above steps into the oil under stirring, adjust the temperature of the reaction pot to 60°C, slowly stir and react in the reaction pot for 2 hours, the pH is at 7.5, and then keep it for 25 minutes ;
[0046] 4) Dissolve 0.4 parts by weight of triglycerin fatty acid ester in rose essence water, then add 1 part by weight of sucrose, stir to make it dissolve, then add 0.5 parts by weight of glycerin and 1 part by weight of ethanol, adjust the temperature to 60°C, then add it into the reaction pot and stir evenly;
[0047] 5)...
Embodiment 2
[0054] A method for preparing rose transparent soap, comprising steps:
[0055] 1) Add 10 parts by weight of oil into the jacketed pot, heat and melt the oil, and control the oil temperature to 83°C;
[0056] 2) dissolving the EDTA of 0.025 parts by weight and the caustic soda of 1.5 parts by weight with 3 parts by weight of rose distilled water, and being mixed with a 30% NaOH solution of 4.525 parts by weight;
[0057] 3) Slowly add the 30% NaOH solution prepared in the above steps into the oil under stirring, adjust the temperature of the reaction pot to 65°C, slowly stir and react in the reaction pot for 2.5 hours, the pH is at 8, and then keep it for 30 minutes ;
[0058] 4) Dissolve 0.6 parts by weight of triglycerin fatty acid ester in rose essence water, then add 2 parts by weight of sucrose, stir to make it dissolve, then add 1 part by weight of glycerin and 1.5 parts by weight of ethanol, adjust the temperature to 65°C, then add it into the reaction pot and stir ev...
Embodiment 3
[0066] A method for preparing rose transparent soap, comprising steps:
[0067] 1) Add 12 parts by weight of oil into the jacketed pot, heat and melt the oil, and control the oil temperature to 85°C;
[0068] 2) Dissolve 0.02-0.03 parts by weight of EDTA and 1.8 parts by weight of caustic soda with 24.17 parts by weight of rose distilled water, and prepare 6 parts by weight of 30% NaOH solution 3-6;
[0069] 3) Slowly add the 30% NaOH solution prepared in the above steps into the oil under stirring, adjust the temperature of the reaction pot to 70°C, slowly stir and react in the reaction pot for 3 hours, the pH is between 8.5, and then keep it warm 35 minutes;
[0070] 4) Dissolve 0.8 parts by weight of triglycerin fatty acid ester in rose essence water, then add 4 parts by weight of sucrose, stir to make it dissolve, then add 1.5 parts by weight of glycerin and 2 parts by weight of ethanol, adjust the temperature to 70°C, then add it into the reaction pot and stir evenly; ...
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