2-dimethylaminoethyl chloride hydrochloride synthesis technology
A technology of dimethylaminoethyl chloride and synthesis process, which is applied in the preparation of amino compounds, the preparation of organic compounds, organic chemistry and other directions, can solve the problems such as being unsuitable for large-scale production, complex production procedures, low production efficiency, etc. Single-pass conversion rate and product yield, overcoming the effect of many processes and improving work efficiency
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[0011] The synthesis technique of the 2-dimethylamino chloroethane hydrochloride of the present embodiment comprises the following steps:
[0012] (1) Using dimethylethanolamine as a raw material, the ice-water bath condition controls the temperature at 12°C to directly carry out chlorination reaction with thionyl chloride;
[0013] (2) Add absolute ethanol to reflux for 2 hours;
[0014] (3) Filter and dry to obtain the finished product.
[0015] The synthesis process of 2-dimethylaminochloroethane hydrochloride does not require cumbersome post-reaction treatment, greatly improves product performance, and is environmentally friendly and pollution-free. The process is easy to implement, low production cost, high synthesis yield, and better The industrialized production of products has been realized.
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