Highly-concentrated essence and preparation method
A flavor and high-power technology, applied in the field of high-power concentrated flavor and preparation, can solve the problems of unstable indicators, high transportation costs, low content, etc., and achieve the effect of good flavor and taste
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Embodiment 1
[0017] 1. Resin cleaning: Soak the resin with 2BV ethanol for 2 hours, then use pure water 3BV / h to clean until there is no ethanol smell, and consume 6BV of pure water.
[0018] 2. Resin adsorption:
[0019] 2-1. Add the essence to be treated, the content of trans-2-hexenal is 214ppm, and the flow rate is controlled at 2BV / h;
[0020] 2-2. Take the permeate at intervals of 1BV to measure the content of trans-2-hexenal, until the concentration of trans-2-hexenal in the permeate of 8BV is 0;
[0021] 2-3. When the permeate reaches 44BV, the concentration of trans-2-hexenal is 225ppm, that is, the resin is saturated, and the essence is stopped.
[0022] 3. Elution:
[0023] 3-1. Use 3BV of pure water to replace the essence in the resin column;
[0024] 3-2. Gradually add 45% ethanol to elute, and the flow rate is controlled at 2BV / h;
[0025] 3-3. Collect the permeate after 0.5BV. When the concentration of trans-2-hexenal in the permeate reaches 8BV, the elution is stopped. ...
Embodiment 2
[0039] 1. Resin cleaning: Soak the resin with 2BV ethanol for 2 hours, then use pure water 3BV / h to clean until there is no ethanol smell, and consume 6BV of pure water.
[0040] 2. Resin adsorption:
[0041] 2-1. Add the essence to be treated, the content of trans-2-hexenal is 214ppm, and the flow rate is controlled at 2BV / h;
[0042] 2-2. Take the permeate at intervals of 1BV to measure the content of trans-2-hexenal, until the concentration of trans-2-hexenal in the permeate of 8BV is 0;
[0043] 2-3. When the permeate reaches 40BV, the concentration of trans-2-hexenal is 230ppm, that is, the resin is saturated, and the essence is stopped.
[0044] 3. Elution:
[0045] 3-1. Use 3BV of pure water to replace the essence in the resin column;
[0046] 3-2. Gradually add 45% ethanol to elute, and the flow rate is controlled at 2BV / h;
[0047] 3-3. Collect the permeate after 0.5BV. When the concentration of trans-2-hexenal in the permeate reaches 10BV, stop elution. When the ...
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