Microcapsule and preparation method thereof
A technology of microcapsules and wall materials, which is applied in the direction of microcapsule preparation, microsphere preparation, tobacco preparation, etc. It can solve the problems affecting the smoking quality and odor of cigarettes, and achieve good film forming, good protection and environmental friendliness Effect
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Embodiment 1
[0026] ①. Take 0.1g of tree moss absolute oil, 800.1g of Tween, 0.1g of sodium tripolyphosphate, add 30ml of deionized water, fully dissolve, and obtain the core material emulsion;
[0027] ②. Take 1.81 g of konjac glucomannan and 0.19 g of chitosan, mix them evenly, add 80 g of 1% acetic acid solution, and fully dissolve to obtain a wall material solution;
[0028] ③. Use a 5# needle to uniformly inject the core material solution into the constantly stirring wall material solution. The stirring speed is 500r / min, and the stirring is continued for 30 minutes; 2.8ml / min, the air velocity is 190m 3 / h, the spray outlet pressure is carried out under the condition of 2.5 atmospheric pressures to carry out spray drying, obtains microcapsules.
Embodiment 2
[0030] ①, add 0.24g of tree moss absolute oil, 800.36g of Tween, 0.18g of sodium tripolyphosphate, add 30ml of deionized water, fully dissolve, and obtain the core material emulsion;
[0031] ②. Take 2.4g of konjac glucomannan and 0.3g of chitosan, mix them evenly, add 67.5g of 1.5% acetic acid solution, fully dissolve, and obtain a wall material solution;
[0032] ③. Use a 5# needle to uniformly inject the core material solution into the constantly stirring wall material solution. The stirring speed is 1500r / min, and the stirring is continued for 60 minutes; 3ml / min, the air velocity is 180m 3 / h, the spray outlet pressure is carried out under the condition of 3 atmospheric pressures to carry out spray drying, obtains microcapsules.
Embodiment 3
[0034] ①. Take 0.375g of tree moss absolute oil, 801.0g of Tween, 0.31g of sodium tripolyphosphate, add 30ml of deionized water, fully dissolve, and obtain the core material emulsion;
[0035] ②. Take 2.5g of konjac glucomannan and 0.5g of chitosan, mix them evenly, add 150g of 2% acetic acid solution, fully dissolve, and obtain a wall material solution;
[0036] ③. Use a 5# needle to uniformly inject the core material solution into the constantly stirring wall material solution. The stirring speed is 2500r / min, and the stirring is continued for 75 minutes; 3.2ml / min, the air velocity is 185m 3 / h, the spray outlet pressure is carried out under the condition of 3.8 atmospheric pressures to carry out spray drying, obtains microcapsules.
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