A kind of catalytic cracking catalyst and its preparation method and application
A catalytic cracking and catalyst technology, used in catalytic cracking, physical/chemical process catalysts, molecular sieve catalysts, etc., can solve the problem of high coke selectivity, achieve high diesel yield, be conducive to diffusion and cracking, and low coke selectivity. Effect
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preparation example Construction
[0023] In the preparation process of the above-mentioned modified aluminum sol, water can be introduced into the reactor through a soluble silicon-containing compound solution, through a chloride solution, through a soluble phosphorus-containing compound solution, by adding water such as deionized water, or through a combination of the above methods Water is introduced into the reactor, preferably, the weight ratio of the water introduced into the reactor before adding the chloride to the soluble silicon-containing compound (calculated as Si element) introduced into the reactor before adding the chloride is 100:0.1- 10, such as 100:1-10 or 100:0.1-5 or 100:0.15-1.4 or 100:0.2-1.3:1.
[0024] The content of silicon (calculated as silicon element) in the modified aluminum sol obtained in the present invention is 0.1-1 wt%, preferably 0.2-0.9 wt%, for example 0.3-0.85 wt%.
[0025] In the preparation process of the above-mentioned modified aluminum sol, the amount of metal alumin...
preparation example
[0069] In the following preparation examples, comparative preparation examples, examples and comparative examples:
[0070] The purity of aluminum chips used is 99.2% by weight, and the purity of aluminum particles is 98.8% by weight; the 1:1 chemically pure hydrochloric acid used is a mixture of 1 volume concentration of 36% by weight chemically pure hydrochloric acid and 1 volume water; the 1:1 chemically pure phosphoric acid used It is a mixture of 1 volume of chemically pure phosphoric acid with a concentration of 85% by weight and 1 volume of water; the rare earth chloride is purchased from Baotou Steel Rare Earth High Technology Co., Ltd., and the rare earth elements are La and Ce.
[0071] The specific surface area, pore volume and average pore diameter were all measured by the low-temperature nitrogen adsorption-desorption method, and the instrument used was the physical and chemical adsorption instrument ASAP2400 of Micro meritics company in the United States; 2 O, Al...
preparation example 1
[0076] This preparation example is used to illustrate the preparation method of the silicon-modified aluminum sol provided by the present invention.
[0077] 286 grams of aluminum chips (calculated as Al), 1481 grams of deionized water and 119 grams of water glass aqueous solution (containing 9.33% by weight of Si element and 4.63% by weight of Na element) were added into the three-necked flask and heated to 60°C. Slowly add 921 ml of 1:1 chemically pure hydrochloric acid into the three-necked flask to make it react with aluminum chips. The addition time of hydrochloric acid is 3 hours; The product was cooled to 60-70°C and filtered to obtain modified aluminum sol SA-1. The residual aluminum chips from the reaction were weighed to be 36 grams, that is, the aluminum excess was 14.8% by weight. After analyzing the modified aluminum sol SA-1, the results are as follows: Al content is 9.0% by weight, Cl content is 6.7% by weight, Si content is 0.41% by weight, Al / Cl (weight ratio...
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