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Organic silicon pouring sealant for LEDs and preparation method for organic silicon pouring sealant

A technology of silicone potting glue and potting glue, which is applied in the directions of adhesives, adhesive additives, non-polymer adhesive additives, etc. To achieve the effect of prolonging life, good adhesion and less corrosiveness

Inactive Publication Date: 2015-11-25
SUZHOU DATONG ADVANCED MATERIAL
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, there are some problems in the use of silicone potting adhesives, such as easy to generate air bubbles during use, which affects the light output rate of LEDs; poor adhesion to materials, which affects the airtightness of potting; deep curing speed Slow, affecting production efficiency; yellowing during use, affecting luminous color, etc.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] The composition and content of the LED silicone potting compound by weight are:

[0028] 1500mPa·S107 glue

100 copies

50mPa·S hydroxy silicone oil

3 copies

100mPa·S methyl silicone oil

5 copies

100mPa·S Methyl-terminated fluorosilicone oil

1 copy

[0029] Orthopropyl silicate

7.0 copies

KH550

1.3 parts

KH560

1.3 parts

catalyst

1.3 parts

[0030] Process formula:

[0031] Base glue: low-viscosity 107 glue, hydroxyl-terminated silicone oil, methyl silicone oil and methyl-terminated fluorosilicone oil are added to the stirring tank according to the formula, stirred at high speed for 30 minutes, and vacuumed to remove air bubbles.

[0032] Auxiliaries: add cross-linking agent, coupling agent and catalyst according to the formula. Stir well.

Embodiment 2

[0034] The composition and content of the LED silicone potting compound by weight are:

[0035] 1500mPa·S107 glue

100 copies

50mPa·S hydroxy silicone oil

3 copies

100mPa·S methyl silicone oil

5 copies

100mPa·S Methyl-terminated fluorosilicone oil

1 copy

Orthopropyl silicate

6.1 copies

KH550

1.3 parts

KH560

0.5 parts

Nantah-42

1.5 servings

catalyst

1.3 parts

[0036] Process formula:

[0037] Base glue: low-viscosity 107 glue, hydroxyl-terminated silicone oil, methyl silicone oil and methyl-terminated fluorosilicone oil are added to the stirring tank according to the formula, stirred at high speed for 30 minutes, and vacuumed to remove air bubbles.

[0038] Auxiliaries: add cross-linking agent, coupling agent and catalyst according to the formula. Stir well.

Embodiment 3

[0040] The composition and content of the LED silicone potting compound by weight are:

[0041] 1500mPa·S107 glue

100 copies

50mPa·S hydroxy silicone oil

3 copies

100mPa·S methyl silicone oil

5 copies

100mPa·S Methyl-terminated fluorosilicone oil

1 copy

[0042] tetraethyl orthosilicate

6.1 copies

KH550

1.3 parts

KH560

0.5 parts

Nantah-42

1.5 servings

catalyst

1.3 parts

[0043] Process formula:

[0044] Base glue: low-viscosity 107 glue, hydroxyl-terminated silicone oil, methyl silicone oil and methyl-terminated fluorosilicone oil are added to the stirring tank according to the formula, stirred at high speed for 30 minutes, and vacuumed to remove air bubbles.

[0045] Auxiliaries: add cross-linking agent, coupling agent and catalyst according to the formula. Stir well.

[0046] The data measured in the above three experiments are as follows:

[0047] ...

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PUM

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Abstract

The invention relates to an organic silicon pouring sealant for LEDs. The organic silicon pouring sealant for LEDs is characterized by comprising the following components (in parts by weight): 90-100 parts of low-viscosity 107 glue, 1-5 parts of hydroxyl end-capping silicone oil, 2-5 parts of methyl silicone oil, 1-5 parts of methyl fluorosilicone oil , 5-10 parts of a cross-linking agent, 1-5 parts of a cross-linking agent and 1-5 parts of a catalyst. The preparation method comprises: adding the low-viscosity 107 glue, the hydroxyl end-capping silicone oil, the methyl silicone oil and the methyl fluorosilicone oil into a stirrer in formula to be stirred for 30 minutes at a high speed, and carrying out vacuum pumping to remove air bubbles to obtain a mixture II; taking the mixture I as base glue; adding the cross-linking agent, the coupling agent and the catalyst according to the formula to be uniformly mixed to obtain a mixture II, and taking the mixture II as an auxiliary gent; and uniformly mixing the base glue with the auxiliary agent in a ratio of the base glue to the auxiliary agent being 10:1, thereby obtaining the organic silicon pouring sealant for LEDs. The organic silicon pouring sealant disclosed by the invention is excellent in bonding force, high in transparency, good in bubble discharge, quick in deep-layer curing and free of yellowing. The organic silicon pouring sealant can be used for protecting the LEDs from invasion of the external environment for a long time.

Description

technical field [0001] The invention relates to a silicone potting glue, in particular to a silicone potting glue for LEDs and a manufacturing method thereof. Background technique [0002] LED is a solid-state semiconductor device that converts electrical energy into visible light. Its luminous efficiency can reach 80%-90%. It is a new type of high efficiency and has the advantages of energy saving, environmental protection and long service life. Long-term exposure of LED chips to harsh and harsh environments is vulnerable to high humidity, high temperature, dust, microorganisms, ray radiation, wind and rain, etc. It is easy to cause a decrease in luminous rate, and serious permanent oxidative damage; followed by external physical Shock and vibration cause physical damage. Therefore, in order to achieve industrial application, it is required to be potted and protected, so that the circuit board and LED are in a stable and safe environment. [0003] Silicone potting adhesiv...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09J183/06C09J11/08C09J11/06
Inventor 任天斌石伟欧杰武传业
Owner SUZHOU DATONG ADVANCED MATERIAL
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