Extractive electrospray ionization mass spectrometry online analysis method for main stream smoke of cigarette
A cigarette mainstream smoke and electrospray technology, applied in the field of online analysis, can solve problems such as ionization difficulties, achieve good repeatability, ensure accuracy, and meet the effects of online analysis and characterization
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[0028] The present invention is further described below in conjunction with accompanying drawing:
[0029] Such as figure 1 As shown, an online analysis method of electrospray extraction and ionization mass spectrometry for mainstream cigarette smoke, the involved devices include: a single-hole smoking machine 3, a two-position three-way solenoid valve 4, a polytetrafluoroethylene tube 5, and a sampling cone 6 , Syringe 7, flow injection pump 8, quartz capillary 9, stainless steel tube 10, etc. Wherein, the single-channel smoking machine 3 is connected with the sampling cone 6 through a two-position three-way solenoid valve 4 , a polytetrafluoroethylene tube 5 . According to the detection needs of cigarette smoke, relevant parameters were optimized through experiments. Wherein, the inner diameter of the polytetrafluoroethylene tube 5 is 4 mm, the hole diameter of the injection cone 6 is 1 mm, the angle between it and the central axis of the mass spectrometry cone 11 is 150°C...
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