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Dibutyl phenylphosphinate flame retardant composition and application method thereof

A technology of dibutyl phenylphosphinate and its application method, which is applied in the field of dibutyl phenylphosphinate flame retardant compositions, can solve the problems of high application cost, high price, flame retardancy and increase of chlorinated paraffin The plasticity is not very good and other problems, to achieve the effect of convenient application, improved compatibility, and reduced application cost

Active Publication Date: 2017-01-11
RES INST OF XIANGCHENG SUZHOU UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Because chlorinated paraffins are cheap and widely used, but the flame retardancy and plasticizing properties of chlorinated paraffins are not very good, so improving the flame retardancy and plasticizing properties of chlorinated paraffins is a hot topic in the plastic processing industry.
It has been found that the flame retardant plasticizer tricresyl phosphate (TCP) can improve the compatibility and flame retardancy of chlorinated paraffin and materials, but its price is expensive and its application cost is high, so it is limited to a certain extent.

Method used

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  • Dibutyl phenylphosphinate flame retardant composition and application method thereof
  • Dibutyl phenylphosphinate flame retardant composition and application method thereof
  • Dibutyl phenylphosphinate flame retardant composition and application method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030] Example 1 Add different proportions of PPDB and CP52 to polyvinyl chloride, stir evenly, extrude a sample strip with a diameter of about 3 mm at melting temperature with an XJ-01 extruder, and measure its The limiting oxygen index, the results are shown in Table 2.

[0031] Table 2 Flame retardant data of PVC compounded by flame retardant PPDB and CP52

[0032]

Embodiment 2

[0033] Example 2 Add different proportions of PPDB, CP52 and STCE to polyvinyl chloride, stir evenly, extrude a sample strip with a diameter of about 3mm at the melting temperature with an XJ-01 extruder, and use a HC900-2 oxygen index tester The limiting oxygen index was measured, and the results are shown in Table 3.

[0034] Table 3 Flame retardant data of PVC compounded by flame retardant PPDB, CP52 and STCE

[0035]

Embodiment 3

[0036] Example 3 Add different proportions of PPDB, CP52 and STDE to polyvinyl chloride, stir evenly, use XJ-01 extruder to extrude a sample with a diameter of about 3mm at the melting temperature, and use HC900-2 oxygen index tester Measure its limiting oxygen index, and the results are shown in Table 4.

[0037] Table 4 Flame retardant data of PVC compounded by flame retardant PPDB, CP52 and STDE

[0038]

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PUM

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Abstract

The invention relates to a dibutyl phenylphosphinate (PPDB) flame retardant composition and an application method thereof. The flame retardant composition is prepared by the steps of compounding one or two of PPDB, chlorinated paraffin-52 (short for CP52), tetrachloroethyl silicate (short for STCE), tetradichloropropyl silicate (short for STDE) or tridichloropropyl phenyl silicate (short for STDPE) according to any ratio, and then, uniformly mixing, wherein the weight parts of both PPDB and CP52 are larger than zero. The flame retardant composition provided by the invention has the advantages of synergistic effect among various elements, good compatibility with materials, high flame-retardant efficiency, low cost and the like, and can be used as a flame retardant for materials such as polyvinyl chloride, polyurethane, unsaturated resin, epoxy resin and the like so as to have favorable application prospects.

Description

technical field [0001] The invention relates to a flame retardant composition of dibutyl phenylphosphinate and an application method thereof. The flame retardant composition can be used as a flame retardant for materials such as polyvinyl chloride, polyurethane, unsaturated resin, and epoxy resin. agent. Background technique [0002] With the continuous advancement of science, polymer materials are more and more used in people's production and life, but due to their flammable characteristics, fires occur frequently, which often pose a serious threat to people's lives and property safety, and promote the development of fire protection. The rapid development of fuel industry. With the enhancement of people's awareness of safety and environmental protection and the continuous promulgation of flame retardant regulations, the research on flame retardants with excellent performance is more urgent, especially the new and efficient flame retardant plasticizers are more popular. Ch...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08K5/00C08K5/5313C08K5/02C08K5/5415C08L27/06
Inventor 刘垚俞春雷王彦林
Owner RES INST OF XIANGCHENG SUZHOU UNIV OF SCI & TECH
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