Microbial water purifying agent for grass shrimp farming water and preparation method of microbial water purifying agent
A microbial reagent, aquaculture water technology, applied in biological water/sewage treatment, chemical instruments and methods, water/sludge/sewage treatment, etc. , the effect of high purification efficiency
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Embodiment 1
[0024] (1) Preparation of magnetic silica spheres with surface-modified C8 and C18 alkyl chains:
[0025] (1-1) Synthesis of Fe by hydrothermal method 3 o 4 Magnetic nanoparticles: 1 g of FeCl 3 ·6H 2 O, dissolved in 30ml of ethylene glycol, adding 4 grams of anhydrous sodium acetate, the reaction temperature is 200 ° C, the reaction time is 12 hours, and Fe is generated 3 o 4 magnetic nanoparticles;
[0026] (1-2) The above Fe 3 o 4 Wash the magnetic nanoparticles with water to remove water-soluble impurities, and then disperse them in 10 g of water to obtain dispersion A. Take a centrifuge tube, add 3 g of the above dispersion A, add 5 ml of 2M HCl solution and sonicate for 8 minutes, and then use a magnet to separate and remove the green color. Clear liquid, then disperse with 10ml water, collect particles with magnet, remove light green clear liquid, disperse ultrasonically with 5 ml 10wt% trisodium citrate solution, let it stand for 2 hours, re-disperse with 5 ml w...
Embodiment 2
[0033] Basically the same as in Example 1, a microbial water purifier for grass shrimp aquaculture water was prepared, the only difference being that the surface modification agent in step (1-4) was different. In Example 2, 0.3 g of dimethyloctylsilane was used as the surface modifier.
Embodiment 3
[0035] Basically the same as in Example 1, a microbial water purifier for grass shrimp aquaculture water was prepared, the only difference being that the surface modification agent in step (1-4) was different. In Example 3, 0.3 g of octadecyltriethoxysilane was used as the surface modifier.
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