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A kind of anti-scratch UV dumb oil for dumb film and preparation method thereof

A technology of scratch resistance and matte oil, applied in the field of UV matt oil, can solve the problems of poor scratch resistance, easy to be scratched, poor adhesion of matte film, etc. Simple and easy method

Active Publication Date: 2016-10-19
东莞宏石功能材料科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, most of the UV matte oils currently on the market are added with inorganic silica-type matting powder. The larger the particle size of this inorganic matting powder, the better the matting efficiency. When the coating film dries, the tiny particles of fumed silica will The surface of the coating film forms a micro-rough surface to reduce the reflection of light to obtain a matte appearance. This kind of inorganic matting powder is only filled in the coating and does not participate in the reaction. Under the action of external force, it is easy to be scratched off, showing poor scratch resistance. In addition, the adhesion on the dumb film is not good

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0041] The preparation method of the anti-scratch UV dumb oil for dumb film of the present embodiment comprises the following preparation steps:

[0042] a. Add 39 parts of 1,6 hexanediol diacrylate and 15 parts of organic matting agent into the mixing pot for pre-dispersion, mix and stir evenly, the stirring speed is 700r / min, and the stirring time is 35min;

[0043] b, then continue to add 5 parts of bisphenol A epoxy acrylic resin, 35 parts of modified polyurethane acrylic resin, 26 parts of tripropylene glycol diacrylate, 3 parts of benzophenone, 4 parts of tertiary amine co-initiator, 4 parts of 2-hydroxy-2-methyl-1-phenylacetone, 4 parts of 1-hydroxycyclohexyl benzophenone, 2 parts of silicone leveling agent, 3 parts of silicone defoamer, mix well, stir Rotating speed is 900r / min, and the time of stirring is 80min, makes oil plant;

[0044] c. Filter the oil with a 320-mesh filter bag to obtain scratch-resistant UV dumb oil for the dumb film.

Embodiment 2

[0046] The preparation method of the anti-scratch UV dumb oil for dumb film of the present embodiment comprises the following preparation steps:

[0047] a. Add 20 parts of 1,6 hexanediol diacrylate and 12 parts of organic matting agent into the stirring pot for pre-dispersion, mix and stir evenly, the stirring speed is 750r / min, and the stirring time is 32min;

[0048] b, then continue to add 8 parts of bisphenol A epoxy acrylic resin, 30 parts of modified polyurethane acrylic resin, 40 parts of tripropylene glycol diacrylate, 2 parts of benzophenone, 5 parts of tertiary amine co-initiator, 3 parts 2-hydroxy-2-methyl-1-phenylacetone, 4 parts 2,4,6-trimethylbenzoyl-diphenylphosphine oxide, 2 parts silicone leveling agent, 2 parts silicone Antifoaming agent, mixing and stirring evenly, the rotating speed of stirring is 850r / min, the time of stirring is 85min, makes oil plant;

[0049] c. Filter the oil with a 320-mesh filter bag to obtain scratch-resistant UV dumb oil for the ...

Embodiment 3

[0051] The preparation method of the anti-scratch UV dumb oil for dumb film of the present embodiment comprises the following preparation steps:

[0052] a. Add 24 parts of 1,6 hexanediol diacrylate and 10 parts of organic matting agent into the mixing pot for pre-dispersion, mix and stir evenly, the stirring speed is 800r / min, and the stirring time is 30min;

[0053] b, then continue to add 10 parts of bisphenol A epoxy acrylic resin, 28 parts of modified polyurethane acrylic resin, 32 parts of tripropylene glycol diacrylate, 3 parts of benzophenone, 3 parts of tertiary amine co-initiator, 3 parts of 1-hydroxycyclohexyl benzophenone, 4 parts of 2,4,6-trimethylbenzoyl-diphenylphosphine oxide, 1 part of silicone leveling agent, 2 parts of silicone defoamer, mix and stir Uniformly, the rotating speed of stirring is 800r / min, and the time of stirring is 90min, makes oil plant;

[0054] c. Filter the oil with a 320-mesh filter bag to obtain scratch-resistant UV dumb oil for the d...

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Abstract

The present invention relates to the field of dummy oil technology, in particular to a scratch-resistant UV dummy oil for a dummy film and a preparation method thereof. The scratch-resistant UV dummy oil for a dummy film of the present invention consists of 5-15 parts of epoxy Acrylic resin, 20-35 parts of modified acrylic resin, 50-65 parts of acrylic monomer, 10-15 parts of photoinitiator, 5-15 parts of matting agent, and 1-5 parts of auxiliary agents; The preparation method of the present invention is as follows: a. adding acrylic monomer and matting agent into a stirring pot for pre-dispersion, mixing and stirring evenly; b. continuing to add epoxy acrylic resin, modified acrylic resin, acrylic acid The monomer, photoinitiator and auxiliary agent are mixed and stirred evenly to obtain the oil; c, the oil can be filtered. The anti-scratch UV matte oil printing of the present invention has better anti-scratch performance on the matte film, and has delicate hand feeling, low matteness, good visual effect, good adhesion and good wear resistance.

Description

technical field [0001] The invention relates to the technical field of UV matte oil, in particular to a scratch-resistant UV matte oil used for matte films and a preparation method thereof. Background technique [0002] With the development of society, people now have higher and higher requirements for the appearance of paper products such as matte effect, and because of its special matte effect, good leveling and good hand feeling, UV matte oil is widely used Applied to various packaging manufacturers. However, most of the UV matte oils currently on the market are added with inorganic silica-type matting powder. The larger the particle size of this inorganic matting powder, the better the matting efficiency. When the coating film dries, the tiny particles of fumed silica will The surface of the coating film forms a micro-rough surface to reduce the reflection of light to obtain a matte appearance. This kind of inorganic matting powder is only filled in the coating and does...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09D163/10C09D175/14C09D7/12
Inventor 林涤非张书磊
Owner 东莞宏石功能材料科技有限公司
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