Phosphorous acid titanium with three-dimensional open-framework structure and preparation method thereof
A technology of skeleton structure and phosphorous acid, which is applied in phosphorous acid, phosphorus oxyacids, chemical instruments and methods, etc., can solve the problems that artificially synthesized titanium phosphite open skeleton materials have not been reported, and achieve the effect of good thermal stability
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0031] A new three-dimensional open framework titanium phosphite structure was synthesized using titanium powder, phosphorous acid, and water as solvents.
[0032] Add 0.24g of titanium powder to a 25mL beaker, continue to add 7mL of water to the beaker and stir for 10 minutes to make it evenly mixed; then add 3.69g of phosphorous acid, continue to stir for 30 minutes to completely dissolve, then transfer the reaction solution to a 15mL poly In a stainless steel kettle lined with tetrafluoroethylene, finally seal the reaction kettle and put it into a 170°C oven for heating for 7 days;
[0033] After the reaction is completed, take out the reaction kettle and let it cool naturally at room temperature; remove the product, wash it repeatedly with deionized water for 6 times, and dry it at 80°C to obtain a new type of three-dimensional open framework titanium phosphate crystal, which is a cuboid Shape, mass about 0.65g.
Embodiment 2
[0035] A new three-dimensional open framework titanium phosphite structure was synthesized with titanium powder, phosphorous acid, hydrofluoric acid, and water as solvents.
[0036] Add 0.24g of titanium powder to a 25mL beaker, continue to add 7mL of water to the beaker and stir for 10 minutes to mix evenly; then add 3.69g of phosphorous acid; continue to stir for 30 minutes to completely dissolve, then add 0.2mL of mass to the beaker The hydrofluoric acid solution with a fraction of 40% was stirred for 30 minutes, then the reaction solution was transferred to a stainless steel kettle lined with 15mL polytetrafluoroethylene, and finally the reaction kettle was sealed and placed in an oven at 170°C for 7 days;
[0037] After the reaction was completed, the reactor was taken out and allowed to cool naturally at room temperature; the product was removed, ultrasonically washed six times with deionized water, and dried at 80°C to obtain a new type of three-dimensional open framewor...
Embodiment 3
[0039] Titanium powder, aqueous solution of phosphorous acid with a mass fraction of 30%, anhydrous piperazine, and water were used as solvents to synthesize a new three-dimensional open framework titanium phosphite structure.
[0040] Add 0.24g of titanium powder into a 25mL beaker, continue to add 7mL of water to the beaker and stir for 10 minutes to make it evenly mixed; then add 6.25mL of an aqueous solution of phosphorous acid with a mass fraction of 30%; continue to stir for 30 minutes, then Add 0.43g of anhydrous piperazine, continue to stir for 30 minutes, then transfer the reaction solution to a stainless steel kettle lined with 15mL polytetrafluoroethylene, and finally seal the reaction kettle and heat it in an oven at 170°C for 7 days;
[0041] After the reaction is completed, take out the reaction kettle and let it cool naturally at room temperature; remove the product, wash it repeatedly with deionized water for 6 times, and dry it at 80°C to obtain a new type of t...
PUM
Property | Measurement | Unit |
---|---|---|
particle diameter | aaaaa | aaaaa |
particle diameter | aaaaa | aaaaa |
quality score | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com