Preparation method of 8-inch <110> magnetic field Czochralski single crystal
A technology of magnetic field Czochralski and single crystal, which is applied in the field of preparation of 8-inch magnetic field Czochralski single crystal, which can solve the problems of low production efficiency and low product quality, achieve cost saving, increase the crystallization rate at one time, and reduce furnace opening and pulling crystal time effect
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Embodiment 1
[0007] The present invention provides a method for preparing an 8-inch magnetic field Czochralski single crystal, which comprises the following steps in sequence: loading material, heating the chemical material, opening the electromagnetic field, stabilizing the temperature, drawing a thinner diameter, releasing the shoulder, retracting the shoulder, and growing with equal diameters , finishing, lifting to cool down and out of the oven. After the temperature is stabilized, the liquid surface temperature of the melted raw material is 1450°C, and the SP value is set to 1300; from the beginning of drawing the thin diameter to the end of the shoulder setting, the SP value is reduced by 100 units; adopt the method of high pulling speed and slow shoulder setting, The pulling speed used when drawing the thin diameter is 400mm / min, and the thin diameter is drawn by the pulling method, the length of the thin diameter is 300mm, and the diameter of the thin diameter is 3-5mm; when the sh...
Embodiment 2
[0010] The present invention provides a method for preparing an 8-inch magnetic field Czochralski single crystal, which comprises the following steps in sequence: loading material, heating the chemical material, opening the electromagnetic field, stabilizing the temperature, drawing a thinner diameter, releasing the shoulder, retracting the shoulder, and growing with equal diameters , finishing, lifting to cool down and out of the oven. After stabilizing the temperature, make the liquid surface temperature of the melted raw materials 1450°C, reduce the SP value by 80 units from the beginning of drawing the thin diameter to the end of the shoulder release, adopt the method of high drawing speed and slow shoulder release, and use the drawing method used when drawing the thin diameter. The speed is 370mm / min, and the thin diameter is drawn by the pulling method, the length of the thin diameter is 230mm, and the diameter of the thin diameter is 3-5mm; when the shoulder is put, the...
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