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Rubber formula and preparation method thereof

A rubber and formula technology, applied in the field of rubber formula and its preparation, can solve the problem of high cost, and achieve the effects of low cost, good comprehensive performance and simple preparation method

Active Publication Date: 2012-12-05
芜湖禾田汽车工业有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Acrylic rubber can solve the problem of high temperature resistance, but the cost of a single acrylate rubber is high, and it is easy to stick to the roll or fall off the roll during mixing, which is difficult to mix

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0014] A kind of rubber formula, its raw material component allocation ratio is shown in Table 1.

[0015] A method for preparing rubber, comprising the steps of:

[0016] A. Raw rubber into the roller: first adjust the roller to the minimum of 0.3-0.5mm, press the stearic acid on the roller, then adjust it to the normal position, add acrylic rubber AR-04T and nitrile rubber according to the formula N240S, cover the roll and guarantee a certain amount of glue;

[0017] B. Rubber compounding: Add zinc oxide, anti-aging agent 4010NA, high wear-resistant carbon black N330 and semi-reinforcing carbon black N774 to the plasticized rubber obtained in step A according to the formula, after the carbon black is all used up , adjust the roller distance to the minimum to 0.3-0.5mm, thin pass 5 times, and park for 22 hours;

[0018] C. Addition of vulcanization system: add sulfur and accelerator TMTD to the mixed rubber prepared in step B according to the formula amount, add potassium s...

Embodiment 2

[0020] A kind of rubber formula, its raw material component allocation ratio is shown in Table 1.

[0021] A method for preparing rubber, comprising the steps of:

[0022] A. Raw rubber into the roller: first adjust the roller to the minimum of 0.3-0.5mm, press the stearic acid on the roller, then adjust it to the normal position, add acrylic rubber AR-04T and nitrile rubber according to the formula N240S, cover the roll and guarantee a certain amount of glue;

[0023] B. Rubber compounding: Add zinc oxide, anti-aging agent 4010NA to the plasticized rubber prepared in step A according to the formula, then add 2 / 3 of the high wear-resistant carbon black N330 and 2 / 3 of half of the formula Reinforcing carbon black N774, add the remaining 1 / 3 of high wear-resistant carbon black N330 and semi-reinforcing carbon black N774 after eating up all the carbon black, eat up all the carbon black, adjust the roller distance to the minimum 0.3-0.5mm, thin pass 5 times parking for 24 hours;...

Embodiment 3

[0026] A kind of rubber formula, its raw material component allocation ratio is shown in Table 1.

[0027] A method for preparing rubber, comprising the steps of:

[0028] A. Raw rubber into the roller: first adjust the roller to the minimum of 0.3-0.5mm, press the stearic acid on the roller, then adjust it to the normal position, add acrylic rubber AR-04T and nitrile rubber according to the formula N240S, cover the roll and guarantee a certain amount of glue;

[0029] B. Rubber compounding: Add zinc oxide, anti-aging agent 4010NA to the plasticized rubber prepared in step A according to the formula, then add 2 / 3 of the high wear-resistant carbon black N330 and 2 / 3 of half of the formula Reinforcing carbon black N774, add the remaining 1 / 3 of high wear-resistant carbon black N330 and semi-reinforcing carbon black N774 after eating up all the carbon black, eat up all the carbon black, adjust the roller distance to the minimum 0.3-0.5mm, thin pass 7 times parking for 22 hours;...

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PUM

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Abstract

The invention discloses a rubber formula and a preparation method thereof. The rubber formula comprises the following raw materials in part by weight: 10-90 parts of acrylic rubber, 10-90 parts of nitrile rubber, 2-6 parts of zinc oxide, 0.5-3 parts of stearic acid, 0.5-3 parts of p-phenylenediamine antioxidant, 30-65 parts of high wear resistant carbon black, 20-75 parts of semi-reinforcing carbon black, 0.2-1 part of sulfur, 0.2-0.8 part of accelerant, 0.5-2 parts of potassium stearate and 1.5-4 parts of sodium stearate, wherein the sum of parts by weight of the acrylic rubber and the nitrile rubber is 100. The preparation method comprises the steps as follows: rolling crude rubber, mixing the rubber and adding a vulcanization system. The rubber prepared by the rubber formula has the advantages of good overall performance and higher mechanical property, oil resistance, high temperature resistance and the like, and is low in cost and suitable for producing an oil resistant sealing element product resistant to the high temperature of 150 DEG C, such as an automobile transmission oil seal gasket; and the preparation method is simple and cannot cause the phenomenon of roll banding or roll release.

Description

technical field [0001] The invention relates to the technical field of rubber manufacturing, in particular to a rubber formula and a preparation method thereof. Background technique [0002] With the development of modern automobile and machinery industry, the demand for heat-resistant and oil-resistant rubber seal products is becoming more and more urgent, and the technical requirements are getting higher and higher. There are many automobile manufacturers and machinery factories that require rubber seals to be used for a long time at a temperature of 150°C. Acrylate rubber can solve the problem of high temperature resistance, but the cost of a single acrylate rubber is high, and it is easy to stick to the roll or fall off the roll during mixing, and it is difficult to mix. Contents of the invention [0003] Aiming at the deficiencies of the prior art, the invention provides a rubber formula and a preparation method thereof. The rubber has good high temperature resistanc...

Claims

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Application Information

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IPC IPC(8): C08L33/04C08L9/02C08K13/02C08K3/22C08K5/09C08K5/18C08K3/04C08K3/06C08K5/098B29B7/38
Inventor 潘琦俊杨建辉
Owner 芜湖禾田汽车工业有限公司
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