Method and system for controlling automatic growth of zone-melt crystal by adopting diameter process
A technology of automatic growth and control area, which is applied in the direction of crystal growth, single crystal growth, chemical instruments and methods, etc. It can solve the problems of long artificial crystal pulling time, poor control of single crystal quality, and large human influence factors, so as to reduce artificial Labor intensity, reduce errors and losses, improve the effect of consistency quality
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[0027] A specific implementation case of automatic growth of a Φ6" zone melting single crystal is given below to further illustrate how the present invention is realized.
[0028] The specific steps of automatic growth of Φ6" zone melting single crystal are as follows:
[0029] (1) Set the growth interval and set the control parameters
[0030] Set the diameter range, taking this implementation as an example, the set range is 50-60mm, 60-70mm, 70-80mm, 80-90mm, 90-100mm, 100-110mm, 110-120 mm, 120-130mm, 130- 140mm, 140-152mm. Then set the control parameter options of each automatic shoulder single crystal diameter interval based on empirical data, for example: in the corresponding set diameter interval 60-70mm, set V lower The falling speed of the single crystal is 3.6mm / min, the power of the generator is 22kw, the rotation speed of the single crystal is 7.5rpm, the rotation speed of the polycrystal is 0.30rpm, R growth The growth rate of the single crystal is 4.0mm / dia ...
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