Improved polymerizable compostions
A technology for polymerizing compositions and mixtures, applied in the field of low VOC polymerizable compositions, can solve problems such as increasing cost, consuming process time, and not wanting
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Embodiment 1
[0019] The reaction product was prepared by the same procedure as described in Comparative Example 1, except that 169 grams of methyl methacrylate was first mixed with polyphosphoric acid before adding 2-hydroxyethyl methacrylate. On a basis excluding methyl methacrylate, the reaction product contained 47.0% by weight monoester and 9.43% by weight diester, corresponding to a monoester:diester molar ratio of 7.64.
Embodiment 2
[0021] The reaction product was prepared by the same procedure as described in Comparative Example 1, except that 302 grams of methyl methacrylate was first mixed with polyphosphoric acid before adding 2-hydroxyethyl methacrylate. On a basis excluding methyl methacrylate, the reaction product contained 47.9% by weight monoester and 7.58% by weight diester, corresponding to a monoester:diester molar ratio of 9.69.
Embodiment 3
[0023] The reaction product was prepared by the same procedure as described in Comparative Example 1, except that 418 grams of methyl methacrylate was first mixed with 200 grams of polyphosphoric acid before adding 218 grams of 2-hydroxyethyl methacrylate. On a basis excluding methyl methacrylate, the reaction product contained 51.0% by weight monoester and 7.24% by weight diester, corresponding to a monoester:diester molar ratio of 10.8.
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