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Fractional distillation apparatus

A rectification and vacuum technology, which is applied in the direction of boiling devices with condensers, distillation separation, chemical instruments and methods, etc., can solve the problems of large energy consumption and large volume, and achieve low energy consumption, reasonable arrangement and low manufacturing cost. low effect

Inactive Publication Date: 2007-08-29
李志平 +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] According to the analysis of the rectification process, in order to realize the rectification separation operation, the rectification tower must have enough layers of trays, so the volume of the traditional rectification device is relatively large; the rectification tower must also introduce the descending liquid flow from the top of the tower and the Generate rising steam flow to establish a vapor-liquid two-phase system, so the energy consumption is relatively large

Method used

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  • Fractional distillation apparatus
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Embodiment Construction

[0021] See Fig. 1, the present invention is a kind of rectifying device, has raw material tank 1, raw material pump and jacket type vacuum vaporizer 3, the bottom of jacket type vacuum vaporizer 3 is provided with heavy component collection tank 31, and jacket 32 An auxiliary heating system 9 is provided, and a sleeve pipe 2 is arranged on the feed pipe of the vacuum vaporization tank 3; A Roots pump 5 is provided, and a condensate collector 6 is connected to the bottom, and each vapor condensation catcher 4 is connected with a refrigerator 71, an oil fraction 73, a heat exchanger 72, an air cooler 74, a liquid storage tank 75, and a subcooler 76 and expansion valve 77 form the cooling circulation system 7. The subcooler 76 is a heat exchange device with a shell and a coil pipe arranged in the shell. The shell and the coil pipe have an inlet and an outlet respectively. The above-mentioned first stage steam The outlet pipe of the gas condensation catcher 41 is connected with th...

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Abstract

The invention relates to a rectify device. It has raw material cans,raw material pump and Jacket vacuum vaporization tank; Also with at least two vapor condensation catchers, Roots pumps set in the intake manifold of the vapor condensation catcher, and condensing collection link the bottom of the vapor condensation catcher, each of the vapor condensation catcher with the refrigerator, heat exchangers and the expansion valve composed cooling circulatory system, the out trachea of first-class vapor condensation catcher connected with the Roots pump of second-class vapor condensation catcher, out trachea of the final one vapor condensation catcher connected with rotary pump, heat exchanger in the different cooling circulatory system installed in a vacuum evaporation tank jacket or installed in raw materials in the tank. This invention's advantages are lower power consumption, simple structure, smaller volume, the distilled production with many varieties, high purity.

Description

technical field [0001] The invention relates to a rectification device. Background technique [0002] The traditional rectification device has a reboiler, a rectification tower, a preheater and a condenser. After the raw material liquid is heated to a specified temperature by the preheater, it is sent to the feed plate of the rectification tower. After the reflux liquid falling from the upper part is combined, it overflows plate by plate, and finally flows into the reboiler at the bottom of the tower; on each plate, the reflux liquid and the rising vapor contact each other to conduct heat and mass transfer processes. During operation, the liquid in the reboiler is continuously vaporized after being heated and decompressed, and rising steam is generated, which passes through each layer of trays in turn, and the steam at the top of the tower enters the condenser to be completely condensed, and part of the condensate is sent back to the top of the tower as The liquid is reflux...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01D3/00B01B1/08
Inventor 李志平范炳喜
Owner 李志平
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