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Preparation of P-type impurity source and doping technique

An impurity source and process technology, applied in semiconductor/solid-state device manufacturing, electrical components, circuits, etc., can solve the problems of large dispersion of electrical parameters, unsatisfactory impurity concentration distribution, complex process, etc., and achieve good dynamic characteristics and high temperature performance. , The effect of ideal impurity concentration distribution and simple diffusion process

Inactive Publication Date: 2007-10-03
SHANDONG NORMAL UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] At present, the one-time P-type doping process in the thyristor production process mainly includes closed-tube aluminum-gallium diffusion and boron-aluminum coating diffusion. Influenced by the quantity and quality of quartz tubes, the diffusion parameters are not easy to adjust, the parameters are highly dispersed, the repeatability is poor, the cycle is long, and the cost is high; the boron-aluminum coating diffusion process, the impurity concentration distribution is not ideal, because the boron impurity distribution is steep, resulting in Large dispersion of electrical parameters, low product qualification rate and excellent product rate, etc.
Due to the shortcomings of the above two diffusion processes, it directly affects the quality and production development of power semiconductor devices, which in turn affects economic benefits

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0014] 1. Preparation of solid aluminum gallium nitrate (double salt) source.

[0015] Put 0.8 grams of high-purity gallium and 0.5 grams of high-purity aluminum powder in the crucible respectively, then add nitric acid that can meet the needs of the complete reaction of high-purity gallium and high-purity aluminum powder, 80 milliliters is enough, and turn on 800 watts Heating on an electric furnace, stirring continuously with a glass rod, the chemical reaction is strong, and finally a solid source of aluminum gallium nitrate (double salt) is generated.

[0016] 2. Preparation of liquid aluminum gallium nitrate source

[0017] Put the solid aluminum gallium nitrate source in a glass, add 50 ml of absolute ethanol, stir continuously with a glass rod, and then perform ultrasonic vibration (ultrasonic wave) to dissolve it fully and quickly to make a liquid aluminum gallium nitrate source, pour it into In a glass bottle, ready to use.

[0018] 3. According to the conventional c...

Embodiment 2

[0024] 1. Preparation of solid aluminum gallium nitrate (double salt) source.

[0025] Put 1.5 grams of high-purity gallium and 1 gram of high-purity aluminum powder in the crucible, and then add nitric acid that can meet the needs of the complete reaction of high-purity gallium and high-purity aluminum powder. Heating on an electric furnace, stirring continuously with a glass rod, the chemical reaction is strong, and finally a solid source of aluminum gallium nitrate (double salt) is generated.

[0026] 2. Preparation of liquid aluminum gallium nitrate source

[0027] Put the solid aluminum gallium nitrate source in a glass, add 100 ml of absolute ethanol, stir continuously with a glass rod, and then perform ultrasonic vibration (ultrasonic wave) to fully dissolve it to make a liquid aluminum gallium nitrate source, pour it into the glass In the bottle, ready to use.

[0028] 3. According to the conventional cleaning process, the N-type silicon wafer (hair sheet) is strictl...

Embodiment 3

[0034] 1. Preparation of solid aluminum gallium nitrate (double salt) source.

[0035] Put 0.8 grams of gallium oxide and 0.6 grams of alumina powder in the crucible respectively, then add nitric acid that can meet the needs of complete reaction of high-purity gallium and high-purity aluminum powder, 130 ml is enough, and put it on a 600-watt electric furnace Heating, stirring constantly with a glass rod, the chemical reaction is strong, and finally a solid source of aluminum gallium nitrate (double salt) is generated.

[0036] 2. Preparation of liquid aluminum gallium nitrate source

[0037] Put the solid aluminum gallium nitrate source in a glass, add 50 ml of absolute ethanol, stir continuously with a glass rod, and then perform ultrasonic vibration (ultrasonic wave) to dissolve it fully and quickly to make a liquid aluminum gallium nitrate source, pour it into In a glass bottle, ready to use.

[0038] 3. According to the conventional cleaning process, the N-type silicon ...

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PUM

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Abstract

First, liquid gallium aluminum nitrate is coated on N type silicon chip. Then, the coated chip is put into diffusion furnace in open pipe system adopted. Under protection of nitrogen atmosphere, P type diffusion is completed through one time of continuous high temperature. Solid gallium aluminum nitrate is generated in reaction vessel through reaction among 0.8-1.5 portion (weight) of gallium in high purity or gallium oxide, 0.5-l portion of aluminum powder in high purity or aluminum oxide and nitric acid. Liquid gallium aluminum nitrate is obtained by dissolving solid gallium aluminum nitrate in absolute ethyl alcohol. Features are: simple technique, easy of operation, even diffusion and better repeatability, better distributed impurity concentration, low cost. Qualification rate is increased to 5-10%.

Description

Technical field: [0001] The invention belongs to the preparation and doping process of a P-type impurity source in the production of power semiconductor devices. Background technique: [0002] At present, the one-time P-type doping process in the thyristor production process mainly includes closed-tube aluminum-gallium diffusion and boron-aluminum coating diffusion. Influenced by the quantity and quality of quartz tubes, the diffusion parameters are not easy to adjust, the parameters are highly dispersed, the repeatability is poor, the cycle is long, and the cost is high; the boron-aluminum coating diffusion process, the impurity concentration distribution is not ideal, because the boron impurity distribution is steep, resulting in The electrical parameters are highly dispersed, and the product qualification rate and excellent product rate are low. Due to the shortcomings of the above two diffusion processes, the quality and production development of power semiconductor dev...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): H01L21/228
Inventor 刘秀喜
Owner SHANDONG NORMAL UNIV
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