Method for preparing field emission display cathode and ZnO nanowire cathode
A nanowire and display technology, applied in nanotechnology, nanotechnology, cold cathode manufacturing, etc., to achieve high efficiency, strong field emission capability, and good operability
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Embodiment 1
[0050] Adopt the novel method for preparing field emission display negative electrode of the present invention to prepare the field emission display negative electrode of ZnO nanowire:
[0051] Step 1: Put 2 grams of zinc powder with a purity of 99.995% on Al 2 o 3 on the ceramic boat, and then put the ceramic boat and zinc powder into the corundum tube together;
[0052] Step 2: Close the corundum tube and then evacuate it. When the vacuum in the corundum tube reaches 1Pa, flow Ar gas into the tube at a flow rate of 70 Sccm;
[0053] Step 3: When the pressure in the corundum tube reaches 0.5MPa, start heating the corundum tube, and raise the temperature to 800°C at a rate of 50°C / min;
[0054] The fourth step: turn off the Ar gas, pass air into the corundum tube, turn off the power supply and vacuum pump after 1 hour of heat preservation, and prepare large-scale ZnO nanowires without any catalyst; see Figure 13 .
[0055] The fifth step: according to the mass ratio, ZnO ...
Embodiment 2
[0061] The first step: put 3 grams of a certain amount of zinc powder (purity: 99.995%) on Al 2 o 3 on the ceramic boat, and then put the ceramic boat and zinc powder into the corundum tube together;
[0062] Step 2: Close the corundum tube and then evacuate it. When the vacuum in the corundum tube reaches 1Pa, flow Ar gas into the tube at a flow rate of 70 Sccm;
[0063] Step 3: When the pressure in the corundum tube reaches 0.5MPa, start heating the corundum tube, and raise the temperature to 800°C at a rate of 50°C / min;
[0064] Step 4: Turn off the Ar gas, pass air into the corundum tube, turn off the power supply and vacuum pump after 1 hour of heat preservation, and prepare ZnO nanowires with a large aspect ratio;
[0065] The fifth step: according to the mass ratio, the ratio of ZnO nanowires: carboxymethyl cellulose is 4:5, weigh the prepared ZnO nanowires, disperse them in hot water with ultrasonic waves for 15 minutes, and after the dispersion is uniform, then weig...
Embodiment 3
[0071] The first step: put 3 grams of zinc powder (99.995%) on Al 2 o 3 on the ceramic boat, and then put the ceramic boat and zinc powder into the corundum tube together;
[0072] Step 2: Close the corundum tube and then evacuate it. When the vacuum in the corundum tube reaches 1Pa, flow Ar gas into the tube at a flow rate of 70 Sccm;
[0073] Step 3: When the pressure in the corundum tube reaches 0.5MPa, start heating the corundum tube, and raise the temperature to 800°C at a rate of 50°C / min;
[0074] Step 4: Turn off the Ar gas, pass air into the corundum tube, turn off the power supply and vacuum pump after 1 hour of heat preservation, and prepare ZnO nanowires with a large aspect ratio;
[0075] The fifth step: according to the mass ratio, the ratio of ZnO nanowires: carboxymethyl cellulose is 3:5, weigh the prepared ZnO nanowires, disperse them in hot water with ultrasonic waves for 15 minutes, and after the dispersion is uniform, then weigh the prepared ZnO nanowires...
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