A fully automatic testing device for impermeability of concrete samples
A testing device, concrete technology, applied in the direction of measuring device, permeability/surface area analysis, suspension and porous material analysis, etc., can solve the problems of manual detection instability, detection accuracy reduction, large manpower and material resources, etc., to eliminate The effects of cumbersome operations and mistakes, avoiding uncertainty, and improving experimental accuracy
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Embodiment 1
[0041] First prepare the detection film 6, the components of the detection film 6 are in grams:
[0042] Ammonium molybdate: 100g-130g,
[0043] Hydrochloric acid with a mass concentration of 18%: 10-13 ml,
[0044] Oxalic acid: 100-120 grams,
[0045] Rosin: 100-150 grams,
[0046] 1-Amino-2-naphthol-4-sulfonic acid: 3 grams,
[0047] Titanium dioxide: 70-90 grams,
[0048] Methanol: 400-500ml
[0049] Sulfurous acid with a mass concentration of 8%: 700-750 ml;
[0050] The preparation is carried out as follows: mix 120 grams of ammonium molybdate, 110 grams of oxalic acid, 4 grams of 1-amino 2-naphthol 4-sulfonic acid, 750 grams of sulfurous acid and 11 milliliters of hydrochloric acid to obtain a precipitate, mix 130 grams of rosin, oxalic acid 110 grams of methanol and 450 milliliters of methanol are made into an intermediate solution, and the precipitate is dissolved in the intermediate solution, and then 70 grams of titanium dioxide are added, stirred and mixed to ...
Embodiment 2
[0074] The difference with the above-mentioned Example 1 is the preparation of the detection film, and its color-changing coating coating solution is carried out according to the following formula:
[0075] Mix 130 grams of ammonium molybdate, 120 grams of oxalic acid, 3 grams of 1-amino 2-naphthol 4-sulfonic acid, 720 sulfurous acid and 10 ml of hydrochloric acid to obtain a precipitate. Mix 150 grams of rosin, 120 grams of oxalic acid and 500 ml of methanol Prepare an intermediate solution, dissolve the precipitate in the intermediate solution, then add 80 grams of titanium dioxide, stir and mix to obtain a color-changing coating solution; apply the color-changing coating solution to the upper end surface of the sample, After drying, the detection film is obtained.
[0076] The detection principle and detection steps are the same as in Example 1.
Embodiment 3
[0078] The difference with the above-mentioned Example 1 is the preparation of the detection film, and its color-changing coating coating solution is carried out according to the following formula:
[0079] Mix 100 grams of ammonium molybdate, 100 grams of oxalic acid, 5 grams of 1-amino 2-naphthol 4-sulfonic acid, 700 grams of sulfurous acid and 13 milliliters of hydrochloric acid to obtain a precipitate. Mix 100 grams of rosin, 100 grams of oxalic acid and 450 milliliters of methanol Prepare an intermediate solution, dissolve the precipitate in the intermediate solution, then add 90 grams of titanium dioxide, stir and mix to obtain a color-changing coating solution; apply the color-changing coating solution to the upper end surface of the sample, After drying, the detection film is obtained.
[0080] The detection principle and detection steps are the same as those in Embodiment 1, and will not be repeated here.
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