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White crystal flower frit, white crystal flower decorative ceramic tile and preparation method thereof

A technology of ceramic tiles and crystal flowers, which is applied in the fields of white crystal flower decorative ceramic bricks and its preparation, crystal flower decorative ceramic tiles, and white crystal flower frits, to achieve natural crystal flowers, good crystallization effects, and improved grades

Active Publication Date: 2020-07-10
MONALISA GRP CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

There are many glazed decorative tiles in the market now, but there are really few that can make consumers shine. Therefore, the development of high value-added glazed tiles will be a new development direction for the ceramic industry.

Method used

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  • White crystal flower frit, white crystal flower decorative ceramic tile and preparation method thereof
  • White crystal flower frit, white crystal flower decorative ceramic tile and preparation method thereof
  • White crystal flower frit, white crystal flower decorative ceramic tile and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0060] Step 1: Press the adobe with ordinary ceramic base material.

[0061] Step 2: kiln drying, the drying time is 1 hour, and the moisture content of the dried billet is controlled within 0.5%.

[0062] Step 3: Spray the surface glaze, the chemical composition of the surface glaze is: IL (loss on ignition): 4.31%, SiO 2 : 50.42%, Al 2 o 3 : 29.41%, Fe 2 o 3 : 0.37%, TiO 2 : 0.07%, CaO: 0.71%, MgO: 0.20%, K 2 O: 5.62%, Na 2 O: 2.58%, P 2 o 5 : 0.26%, ZrO 2 : 6.05%, surface glaze specific gravity 1.44, glaze amount 500g / m 2 .

[0063] Step 4: Drying in a small electric kiln, the temperature of the drying kiln is controlled at 110°C, and the moisture after drying is controlled within 0.5%.

[0064] Step 5: Spray into protective glaze, specific gravity 1.21, glaze amount 280g / m 2 ; The chemical composition of the protective glaze is as follows by weight percentage: IL: 5.31%; SiO 2 : 56.19%; Al 2 o 3 : 17.50%; Fe 2 o 3 : 0.17%; BaO: 1.66%; CaO: 6.09%; MgO: 2.11%...

Embodiment 2

[0075] Basically the same as Example 1, the difference is:

[0076] Step 6: Sprinkle the white crystal flower frit, the spreading amount is 800g / m 2 . The chemical composition of the frit includes by mass percentage: IL: 0.44%; SiO 2 : 41.53%; Al 2 o 3 : 26.78%; Fe 2 o 3 : 0.16%; TiO 2 : 0.15%; CaO: 3.98%; MgO: 1.64%; K 2 O: 2.78%; Na 2 O: 1.73%; ZrO 2 : 3.98%; CeO 2 : 6.98%; ZnO: 5.98%; BaO: 2.45%; PbO: 0.97%; As 2 o 3 : 0.45%. The particle gradation of the frit is as follows: 40 mesh or less: 17%; 40 mesh to 60 mesh: 48%; 60 mesh to 80 mesh: 26%; 80 mesh to 100 mesh: 7%; 100 mesh or more: 2% . The thickness of the effective glaze layer finally obtained from the white crystal flower frit is 0.4mm.

[0077] Step 7: Spray glue fixative on the glaze cabinet. The glue fixative is obtained by mixing and diluting glue and water according to the mass ratio of 3:1, and the glue is purchased from Yidajia Company. The spraying amount of the glue fixing agent is 200g / m ...

Embodiment 3

[0080] Basically the same as Example 1, the difference is:

[0081] Step 6: Sprinkle white crystal flower frit, and its spreading amount is 1000g / m 2 . The chemical composition of the frit includes by mass percentage: IL: 0.52%; SiO 2 : 41.45%; Al 2 o 3 : 26.46%; Fe 2 o 3 : 0.09%; TiO 2 : 0.12%; CaO: 3.99%; MgO: 1.73%; K 2 O: 2.08%; Na 2 O: 2.15%; ZrO 2 : 4.45%; CeO 2 : 8.01%; ZnO: 6.02%; BaO: 2.01%; PbO: 0.83%; As 2 o 3 : 0.09%. The particle gradation of the frit is: 40 mesh or less: 17%; 40 mesh to 60 mesh: 45%; 60 mesh to 80 mesh: 28%; 80 mesh to 100 mesh: 8%; 100 mesh or more: 2% . Finally, the thickness of the effective glaze layer obtained from the white crystal flower frit is 0.5 mm.

[0082] Step 7: Spray glue fixative on the glaze cabinet. The glue fixative is obtained by mixing and diluting glue and water according to the mass ratio of 3:1, and the glue is purchased from Yidajia Company. The spraying amount of the glue fixing agent is 250g / m 2 . In...

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Abstract

The invention discloses a white crystal flower frit, a white crystal flower decorative ceramic tile and a preparation method thereof. The white crystal flower frit comprises the following chemical components in percentage by mass: 0.34%-0.52% of ignition loss, 40.89%-42.10% of SiO2, 26.46%-28.31% of Al2O3, 0.09%-0.25% of Fe2O3, 0.12%-0.16% of TiO2, 3.98%-4.62% of CaO, 1.64%-2.28% of MgO, 2.08%-3.95% of K2O, 1.73%-2.15% of Na2O, 3.78%-4.45% of ZrO2, 6.98%-8.01% of CeO2, 5.98%-7.78% of ZnO, 2.01%-2.78% of BaO, 0.83%-1.07% of PbO, and 0.09%-1.12% of As2O3.

Description

technical field [0001] The invention relates to a crystal flower decorative ceramic brick, in particular to a white crystal flower frit, a white crystal flower decorative ceramic brick and a preparation method thereof, belonging to the technical field of ceramic brick production and decoration. Background technique [0002] With the improvement of living standards and the rapid development of technology, people pay more and more attention to interior decoration, not only requiring high-quality decoration materials, but also requiring them to have ornamental value. Now there are many glazed decorative tiles in the market, but there are really few that can make consumers shine. Therefore, the development of high value-added glazed tiles will be a new development direction for the ceramic industry. Contents of the invention [0003] In order to overcome the deficiencies of the prior art, the object of the present invention is to provide a white crystal flower frit, a white cr...

Claims

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Application Information

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IPC IPC(8): C03C8/12C04B41/89
CPCC03C8/12C04B41/52C04B41/89C04B41/5022C04B41/0072C04B41/4539
Inventor 潘利敏杨元东覃增成王贤超程科木
Owner MONALISA GRP CO LTD
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