Preparation process of ultrahigh-energy-storage activated carbon material
A preparation process, activated carbon technology, applied in inorganic chemistry, non-metallic elements, carbon compounds, etc., can solve the problems of low specific surface area and adsorption performance of activated carbon, electric energy storage and specific surface area that cannot meet the development needs of high-energy automobile batteries, etc.
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Embodiment 1
[0016] First, the polyurethane material and urotropine are added to the high-speed crusher in a ratio of 100:3 by weight and crushed into a powder of 100-325 mesh; the cellulose and the fine powder with a weight of 8% of the weight of the polyurethane material are added together The high-speed mixer is used for mixing, and after mixing evenly, the output material automatically enters the twin-screw extruder for extrusion and granulation. The parameters of the extruder are: internal temperature 150 ° C, back pressure 2 MPa, die hole diameter 4 mm; The cooled pellets are input into the carbonization activation furnace for carbonization activation, and then the furnace temperature is raised to 300°C at a heating rate of 5°C / min. Heating rate Raise the furnace temperature to 650°C and keep the constant temperature for 1.5 hours to carbonize the pellets. After closing the nitrogen gas, mix carbon dioxide and water vapor according to the volume ratio of 1.4:1. The ratio of activator...
Embodiment 2
[0018] First, the polyurethane material and urotropine are added to the high-speed crusher in a ratio of 100:8 by weight and crushed into 100-325 mesh powder; the weight is 5% of the weight of the polyurethane material and the fine powder is added together The high-speed mixer is used for mixing, and after mixing evenly, the output material automatically enters the twin-screw extruder for extrusion and granulation. The parameters of the extruder are: internal temperature 250 ° C, back pressure 16 MPa, die hole diameter 1 mm; The cooled pellets are input into the carbonization activation furnace for carbonization activation, and then the furnace temperature is raised to 350°C at a heating rate of 5°C / min, and then nitrogen gas is introduced to keep the constant temperature for 1.5 hours to carbonize the pellets, and then the pellets are carbonized at a heating rate of 3°C / min. Heating rate Raise the furnace temperature to 640°C and keep it at a constant temperature for 1.5 hours...
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