Novel compound repellent for apolygus lucorum as well as preparation method and application thereof
A technology for compound repelling and green stink bug, applied in animal repellents, botanical equipment and methods, applications, etc., can solve problems such as unpleasantness, reduce irritating pungent odor, ensure repellent effect, and maintain efficacy. long term effect
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Embodiment 1
[0025] The indoor repellent effect test uses such as figure 1 The device shown (810mm×250mm×250mm) is composed of 5 sub-chambers, and the partitions between each sub-chamber are evenly distributed with many round holes, and the circular holes on the partitions on both sides are gradually reduced from the most middle sub-chamber (30mm to 10mm ), put the device into a behavior observation box (100cm×100cm×80cm), and the behavior observation box is a stainless steel shell. The indoor temperature is 26-28°C, and the relative humidity is 60%-70%.
[0026] Before the test, starvation treatment was carried out for 4 hours to the adults of Lygus lucidum (only a cotton ball dipped in pure water was provided), and then they were used for the behavior selection test. The lure in room A is obtained by mixing dimethyl disulfide and dodecanal, the ratios are 10:1, 5:1, 3:1, 2:1, 1:1, 1:2, 1:3, 1 :5 and 1:10 (mass ratio), and then dissolved in liquid paraffin oil, the final concentration o...
Embodiment 2
[0029] Preparation of compound repellent of Lygus viridiensis and construction of sustained-release system: the effective components of repellent dimethyl disulfide and dodecanal (mass ratio 1:10) mixture (adding 0.1% BHT for anti-oxidation) After diluting the liquid paraffin oil at 1:10, 1:20, 1:40 and 1:80 (volume ratio), pipette 1.0 mL into 2.0 mL polyethylene slow-release vials and seal them, and repeat 3 times. Place the sealed vials outdoors. On the 1st, 15th, 30th, 45th, and 60th day after storage, take out the polyethylene slow-release vials, collect volatiles with a gas collection device for 1 hour, and rinse with 400ul chromatographically pure n-hexane for adsorption. Put the eluate into a 1.5ml standard sample bottle and store it in a refrigerator at 4°C for subsequent quantitative analysis, and the polyethylene slow-release vial should continue to be placed outdoors.
[0030] The degradation of effective components of the repellent diluted in different concentratio...
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