Method for rapidly identifying year of dried tangerine or orange peel and citrus chachiensis hortorum by virtue of infrared spectroscopy
A technology of infrared spectroscopy and tangerine peel, which is applied in the field of infrared spectroscopy and year identification of the quality of tangerine peel and tangerine peel medicinal materials, can solve the problems of low identification accuracy and strong human subjectivity in character identification, and achieve uniform thickness, high medicinal value, and shape neat effect
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Embodiment 1
[0020] 1. Drying and sifting: take the medicinal material (sample A) of tangerine peel to be identified, break the whole tangerine peel sample into small pieces and put it into a tangerine peel grinder for crushing, grind the crushed sample and pass it through a 300-mesh sieve. The 300-mesh tangerine peel sample was placed in a weighing bottle and dried in a drying oven at a temperature of 60 °C to constant weight.
[0021] 2. Tablet compression: Mix the original medicinal material sample of tangerine peel after constant weight with KBr crushed crystals in a ratio of 1:100, grind until the fine powder is uniform, and then compress into tablets.
[0022] 3. Tablet samples were scanned in the infrared spectrum in the range of 4000 - 400 cm-1 ( Figure 6 ), and compared the spectra to the library, the ratio of the intensity of the 1742 cm-1 absorption peak to the intensity of the base peak at 1635 cm-1 was 0.38, which was greater than 0.20.
[0023] 4. Sample A volatile oil ...
Embodiment 2
[0026] 1. Drying and sifting: Take the medicinal material (sample B) of tangerine peel to be identified, break the whole tangerine peel sample into small pieces and put it into a tangerine peel grinder for crushing, grind the crushed sample and pass it through a 200-mesh sieve. Put the 200-mesh tangerine peel sample in a weighing bottle and dry it in a normal temperature vacuum oven (vacuum degree less than 0.1 MPa) to constant weight.
[0027] 2. Tablet compression: Mix the original medicinal material sample of tangerine peel after constant weight with KBr crushed crystals in a ratio of 1:100, grind until the fine powder is uniform, and then compress into tablets.
[0028] 3. Tablet samples were scanned in the infrared spectrum in the range of 4000 - 400 cm-1 ( Figure 7 ), and compared the spectra to the library, the ratio of the intensity of the 1742 cm-1 absorption peak to the intensity of the 1635 cm-1 base peak was 0.15, which was less than 0.20.
[0029] 4. Specime...
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