Hemispherical shell-like porous gold micro-nano structure and its preparation method and application
A technology of micro-nano structure and hemispherical shell, which is applied in the direction of nanotechnology, nanotechnology, nanotechnology for materials and surface science, etc., can solve the problems of complexity, reduction of SERS activity, difficulty in obtaining SERS, etc., to reduce damage, SERS The effect of high activity and high SERS activity
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Embodiment 1
[0035] The concrete steps of preparation are:
[0036] First, put the graphite sheet as the anode and the conductive substrate as the cathode in the silver electrolyte, at 100μA / cm 2 Electrodeposition at a constant current for 200min; wherein, the conductive substrate is an indium tin oxide glass substrate, and the silver electrolyte is a mixed solution of 0.2g / L silver nitrate aqueous solution and 50g / L citric acid aqueous solution, and the Silver Nanoparticles Assembled Micro-Hemispheres on Conductive Substrates. After cleaning the conductive substrate with micron hemispheres assembled by silver nanoparticles on it with deionized water once, place it in the gold electrolyte and let it stand for 60 minutes, take it out and wash it once with deionized water , dried at 40°C; wherein, the gold electrolyte is a mixture of 0.3g / L chloroauric acid aqueous solution and 50g / L sodium chloride aqueous solution, which is similar to figure 1 The shown hemispherical shell-like porous go...
Embodiment 2
[0038] The concrete steps of preparation are:
[0039] First place graphite sheet as anode and conductive substrate as cathode in silver electrolyte, at 325μA / cm 2 Electrodepositing at a constant current for 158min; wherein, the conductive substrate is an indium tin oxide glass substrate, and the silver electrolyte is a mixed solution of 1g / L silver nitrate aqueous solution and 40g / L citric acid aqueous solution, and the silver electrolyte attached on it is obtained. Nanoparticle-Assembled Microhemispheres on Conductive Substrates. After cleaning the conductive substrate with micron hemispheres assembled by silver nanoparticles with deionized water for 2 times, place it in the gold electrolyte and let it stand for 95 minutes, take it out and clean it with deionized water for 2 times , dried at 45°C; wherein, the gold electrolyte is a mixture of 1g / L chloroauric acid aqueous solution and 40g / L sodium chloride aqueous solution, which is similar to figure 1 The shown hemispheri...
Embodiment 3
[0041] The concrete steps of preparation are:
[0042] First, put the graphite sheet as the anode and the conductive substrate as the cathode in the silver electrolyte, at 550μA / cm 2Electrodepositing at a constant current for 115min; wherein, the conductive substrate is an indium tin oxide glass substrate, and the silver electrolyte is a mixed solution of 5g / L silver nitrate aqueous solution and 25g / L citric acid aqueous solution, and the silver electrolyte attached on it is obtained. Conductive substrates for nanoparticle-assembled microhemispheres. After cleaning the conductive substrate with micron hemispheres assembled by silver nanoparticles with deionized water for 2 times, place it in the gold electrolyte and let it stand for 130 minutes, take it out and clean it with deionized water for 2 times , dried at 50°C; wherein, the gold electrolyte is a mixed solution of 3g / L chloroauric acid aqueous solution and 25g / L sodium chloride aqueous solution, prepared as figure 1 T...
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