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Essence and its preparation process of tree moss extract

A technology of tree moss extract and essence, which is applied in the directions of essential oils/spice, fat production, etc., can solve problems such as non-industrial mass production, etc., and achieve the effect of easy industrial mass production

Active Publication Date: 2019-08-20
CHINA TOBACCO JIANGSU INDAL
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Chinese patent CN 103333743 A discloses a kind of moss-like fragrance compounded with orcinol monomethyl ether, bifurcated lentilin monomethyl ether, ethyl lentilate, methyl lentilate, etc. The characteristic flavor formula, but some of the monomer fragrances, such as ethyl echinacea, have not yet been mass-produced industrially, and are currently obtained by means of separation from moss fragrance fragrance

Method used

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  • Essence and its preparation process of tree moss extract
  • Essence and its preparation process of tree moss extract

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] Weigh a total of 200g of tree moss extract and absolute ethanol with a mass ratio of 1:4, disperse it into a uniform system through a homogenizer, degas the obtained system by ultrasonic for 4 minutes, and then add it to the liquid bottle of the wiped-film molecular distillation device , turn on the cooling circulating water, set the temperature of the first-stage and second-stage condensed water to 2°C, use liquid nitrogen to condense the third stage, adjust the parameters of the device to the distillation temperature of 50°C, and the speed of the wiper to 150r / min, when the absolute pressure is 5Pa, start feeding at a rate of 3ml / min, and collect the first-order, second-order, and third-stage fractions respectively.

[0024] The essence of the function of the tree moss extract, each component in terms of mass percentage is: 10% of the molecular distillation first-stage fraction of the tree moss extract, 44% of the second-stage fraction of the molecular distillation of...

Embodiment 2

[0026]Weigh a total of 200g of tree moss extract and absolute ethanol with a mass ratio of 1:4, disperse it into a uniform system through a homogenizer, degas the obtained system by ultrasonic for 4 minutes, and then add it to the liquid bottle of the wiped-film molecular distillation device , turn on the cooling circulating water, set the temperature of the first-stage and second-stage condensed water to 2°C, use liquid nitrogen to condense the third stage, adjust the parameters of the device so that the distillation temperature is 80°C, and the speed of the wiper is 200r / min, when the absolute pressure is 2.5Pa, start feeding at a rate of 3ml / min, and collect the first-stage, second-stage, and third-stage fractions respectively.

[0027] The essence of the function of the tree moss extract, each component in terms of mass percentage is: 14% of the molecular distillation first-stage fraction of the tree moss extract, 28% of the second-stage fraction of the molecular distillat...

Embodiment 3

[0029] Weigh a total of 200g of tree moss extract and absolute ethanol with a mass ratio of 1:4, disperse it into a uniform system through a homogenizer, degas the obtained system by ultrasonic for 4 minutes, and then add it to the liquid bottle of the wiped-film molecular distillation device , turn on the cooling circulating water, set the temperature of the first-stage and second-stage condensed water to 2°C, use liquid nitrogen to condense the third stage, adjust the parameters of the device to the distillation temperature of 120°C, and the speed of the wiper to 200r / min, when the absolute pressure is 10Pa, start feeding at a rate of 3ml / min, and collect the first-stage, second-stage, and third-stage fractions respectively.

[0030] The essence of the function of the tree moss extract, the components in terms of mass percentages are: the first molecular distillation fraction of the tree moss extract is 17%, the second stage fraction of the tree moss extract molecular distil...

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Abstract

The invention provides an essence with a tree moss extract function and a preparation technology thereof .The essence is prepared from, by mass, 10-30% of molecular distillation first-stage fraction of tree moss extract, 15-50% of molecular distillation second-stage fraction of tree moss extract, 10-40% of molecular distillation third-stage fraction of tree moss extract, 0.2-2% of geranyl acetate, 0.5-2.5% of cis-3-hexenyl acetate, 0.4-2% of menthyl acetate, 0.6-2.2% of cinnamyl acetate, 0.1-1.5% of 1% bread ketone, 0.8-5% of 1% damascenone, 0.2-1.5% of 1% 2,3,5-trimethyl pyrazine, 0.9-3% of 1% geranium oil, 15-40% of propylene glycol and 10-40% of edible alcohol .The fractions for essence compounding are derived from the tree moss extract and obtained through a molecular distillation technology, no waste liquid or waste gas is produced in the whole process, preparation is safe and environmentally friendly, and industrial batch production is easy to achieved; the natural property of the essence is ensured to the greatest possible, and the natural fragrance feature is provided for the product .

Description

technical field [0001] The invention relates to an essence with the function of tree moss extract and a preparation process thereof. Background technique [0002] Treemoss concrete is made from a tea-stained lichen plant belonging to the genus Usneaceae, which belongs to the Usneaceae genus, and is obtained through certain processing techniques such as petroleum ether or benzene extraction. Both tree moss extract and oakmoss products are natural spices with typical moss fragrance characteristics. They are often used as tobacco additives and natural fragrance raw materials for daily cosmetics. The price of tree moss products is relatively cheap, so they are often used as oakmoss. The substitute of moss products occupies an important position in the international market of natural spices. [0003] The composition of moss extract is complex, and its quality and composition are not only related to plant species, but also vary with soil composition, climatic conditions, growing ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C11B9/00
Inventor 朱怀远庄亚东万敏张媛曹毅尤晓娟沈晓晨韩开冬何红梅刘献军
Owner CHINA TOBACCO JIANGSU INDAL
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