Nitraria branch and leaf extract
A technology of extract and Nitraria, applied in the direction of drug combination, plant raw materials, plant/algae/fungus/moss components, etc., can solve the problems of low efficiency, high extraction cost, incomplete recovery of organic solvents, etc., and achieve simple operation Effect
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Embodiment 1
[0040] 1. Cleaning: select 10kg of mature Nitraria branches and leaves, sieve out the sediment, and wash with water;
[0041] 2. Drying: Dry the cleaned Nitraria branches and leaves at 15°C for 15 hours at low temperature;
[0042] 3, crushing: the Nitraria branches and leaves obtained in step 2 are ultrafinely pulverized to obtain Nitraria branches and leaves powder;
[0043] 4. Extraction: Add 5 times the amount of 70% ethanol to the Nitraria branch and leaf powder obtained in step 3 for ultrasonic extraction for 1 hour, stir with a stirrer during this period, obtain filtrate I and filter residue I after filtration, and use filter residue I again for 7 times A large amount of 70% ethanol was refluxed and extracted for 1 h, and the filtrate II and filter residue II were obtained after filtration, the filtrate I and the filtrate II were combined, and concentrated under reduced pressure to obtain the crude extraction part of the total flavonoids of the branches and leaves of Ni...
Embodiment 2
[0047] 1. Cleaning: select 10kg of mature Nitraria branches and leaves, sieve out the sediment, and wash with water;
[0048] 2. Drying: Dry the cleaned Nitraria branches and leaves at 20°C for 15 hours at low temperature;
[0049] 3, crushing: the Nitraria branches and leaves obtained in step 2 are ultrafinely pulverized to obtain Nitraria branches and leaves powder;
[0050]4. Extraction: Add 8 times the amount of 70% ethanol to the powder of Nitraria thorn leaves obtained in step 3 for ultrasonic extraction for 1 hour, stir with a stirrer during this period, obtain filtrate I and filter residue I after filtration, and use filter residue I again for 6 times A large amount of 80% ethanol was refluxed and extracted for 1 h, and the filtrate II and filter residue II were obtained after filtration, the filtrate I and the filtrate II were combined, and concentrated under reduced pressure to obtain the crude extraction part of the total flavonoids of the branches and leaves of Nit...
Embodiment 3
[0054] 1. Cleaning: select 10kg of mature Nitraria branches and leaves, sieve out the sediment, and wash with water;
[0055] 2. Drying: Dry the cleaned Nitraria branches and leaves at 15°C for 20 hours at low temperature;
[0056] 3, crushing: the Nitraria branches and leaves obtained in step 2 are ultrafinely pulverized to obtain Nitraria branches and leaves powder;
[0057] 4. Extraction: Add 5 times the amount of 70% ethanol to the Nitraria branch and leaf powder obtained in step 3 for ultrasonic extraction for 1.5 hours, stir with a stirrer during this period, obtain filtrate I and filter residue I after filtration, and use filter residue I again for 7 Doubling the amount of 65% ethanol for reflux extraction for 1.5 h, after filtration, filtrate II and filter residue II were obtained, the filtrate I and filtrate II were combined, concentrated under reduced pressure to obtain the crude extraction part of the total flavonoids of the branches and leaves of Nitraria japonica;...
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